Technology Process of C67H66FN6O9PS
There total 7 articles about C67H66FN6O9PS which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
tetrachloromethane;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: trimethylsilyl trifluoromethanesulfonate / acetonitrile / 73 h / 20 - 65 °C
2: water; ammonia / methanol / 16 h / 20 °C
3: chloro-trimethyl-silane; pyridine / 0 - 25 °C
4: pivaloyl chloride; pyridine / -30 - 0 °C
5: tetrachloromethane
With
pyridine; chloro-trimethyl-silane; trimethylsilyl trifluoromethanesulfonate; ammonia; water; pivaloyl chloride;
In
methanol; tetrachloromethane; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: n-butyllithium / tetrahydrofuran; hexanes / 0.5 h / -78 °C
1.2: 0.75 h
2.1: trimethylsilyl trifluoromethanesulfonate / acetonitrile / 73 h / 20 - 65 °C
3.1: water; ammonia / methanol / 16 h / 20 °C
4.1: chloro-trimethyl-silane; pyridine / 0 - 25 °C
5.1: pivaloyl chloride; pyridine / -30 - 0 °C
6.1: tetrachloromethane
With
pyridine; n-butyllithium; chloro-trimethyl-silane; trimethylsilyl trifluoromethanesulfonate; ammonia; water; pivaloyl chloride;
In
tetrahydrofuran; methanol; tetrachloromethane; hexanes; acetonitrile;