2,4,6-tris(4-((tert-butyldimethylsilyl)oxy)-5-methoxy-2-methylphenyl)-1,3,5,2,4,6-trioxatriborinane

Base Information

Chemical Name:2,4,6-tris(4-((tert-butyldimethylsilyl)oxy)-5-methoxy-2-methylphenyl)-1,3,5,2,4,6-trioxatriborinane
CAS No.:1453107-64-6
Molecular Formula:C₄₂H₆₉B₃O₉Si₃
Molecular Weight:834.694
Hs Code.:

Synonyms:2,4,6-tris(4-((tert-butyldimethylsilyl)oxy)-5-methoxy-2-methylphenyl)-1,3,5,2,4,6-trioxatriborinane

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Chemical Property of 2,4,6-tris(4-((tert-butyldimethylsilyl)oxy)-5-methoxy-2-methylphenyl)-1,3,5,2,4,6-trioxatriborinane

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Technology Process of 2,4,6-tris(4-((tert-butyldimethylsilyl)oxy)-5-methoxy-2-methylphenyl)-1,3,5,2,4,6-trioxatriborinane

There total 3 articles about 2,4,6-tris(4-((tert-butyldimethylsilyl)oxy)-5-methoxy-2-methylphenyl)-1,3,5,2,4,6-trioxatriborinane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.2%

: 1453107-63-5
(4-bromo-2-methoxy-5-methylphenoxy)(tert-butyl)dimethylsilane

: 1453107-64-6
2,4,6-tris(4-((tert-butyldimethylsilyl)oxy)-5-methoxy-2-methylphenyl)-1,3,5,2,4,6-trioxatriborinane

Guidance literature:: With n-butyllithium; Triisopropyl borate; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol402302k

Reference yield:

: 1195-09-1
5-methyl-2-methoxyphenol

: 1453107-64-6
2,4,6-tris(4-((tert-butyldimethylsilyl)oxy)-5-methoxy-2-methylphenyl)-1,3,5,2,4,6-trioxatriborinane

Guidance literature:: Multi-step reaction with 3 steps

1: N-Bromosuccinimide / acetic acid / Inert atmosphere

2: 1H-imidazole / dichloromethane / Inert atmosphere

3: Triisopropyl borate; n-butyllithium / tetrahydrofuran / -78 - 20 °C / Inert atmosphere

With 1H-imidazole; N-Bromosuccinimide; n-butyllithium; Triisopropyl borate; In tetrahydrofuran; dichloromethane; acetic acid;
DOI:10.1021/ol402302k

Reference yield:

: 40992-09-4
4-bromo-2-methoxy-5-methylphenol

: 1453107-64-6
2,4,6-tris(4-((tert-butyldimethylsilyl)oxy)-5-methoxy-2-methylphenyl)-1,3,5,2,4,6-trioxatriborinane

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole / dichloromethane / Inert atmosphere

2: Triisopropyl borate; n-butyllithium / tetrahydrofuran / -78 - 20 °C / Inert atmosphere

With 1H-imidazole; n-butyllithium; Triisopropyl borate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol402302k