C₁₈H₁₃Br₂NO₂S

Base Information

Chemical Name:C₁₈H₁₃Br₂NO₂S
CAS No.:1312611-67-8
Molecular Formula:C₁₈H₁₃Br₂NO₂S
Molecular Weight:467.181
Hs Code.:

C<sub>18</sub>H<sub>13</sub>Br<sub>2</sub>NO<sub>2</sub>S

Synonyms:C₁₈H₁₃Br₂NO₂S

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Chemical Property of C₁₈H₁₃Br₂NO₂S

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Technology Process of C₁₈H₁₃Br₂NO₂S

There total 8 articles about C₁₈H₁₃Br₂NO₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1312609-99-6
C₁₈H₁₅NO₂S

: 1312611-67-8
C₁₈H₁₃Br₂NO₂S

Guidance literature:: With bromine; acetic acid; In chloroform; at 70 ℃;

Reference yield:

: 90-04-0
2-methoxy-phenylamine

: 1312611-67-8
C₁₈H₁₃Br₂NO₂S

Guidance literature:: Multi-step reaction with 8 steps

1.1: triethylamine / 3 h / 0 - 20 °C

2.1: Lawessons reagent / toluene / 3 h / 110 °C / Inert atmosphere

3.1: potassium hexacyanoferrate(III); sodium hydroxide / ethanol; water / 0.83 h / 90 °C

4.1: aluminum (III) chloride / carbon disulfide / 1.5 h / Reflux

5.1: aluminum (III) chloride / 1,2-dichloro-ethane / 5 h / Inert atmosphere; Reflux

5.2: Cooling with ice

6.1: triethylamine / dichloromethane / 2 h / 0 °C / Inert atmosphere

7.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 80 °C / Inert atmosphere

8.1: bromine; acetic acid / chloroform / 70 °C

With Lawessons reagent; aluminum (III) chloride; bromine; sodium carbonate; acetic acid; triethylamine; sodium hydroxide; potassium hexacyanoferrate(III); aluminum (III) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In carbon disulfide; ethanol; dichloromethane; chloroform; water; 1,2-dichloro-ethane; toluene; 7.1: Suzuki Coupling;

Reference yield:

: 93-26-5
2-methoxyacetanilide

: 1312611-67-8
C₁₈H₁₃Br₂NO₂S

Guidance literature:: Multi-step reaction with 7 steps

1.1: Lawessons reagent / toluene / 3 h / 110 °C / Inert atmosphere

2.1: potassium hexacyanoferrate(III); sodium hydroxide / ethanol; water / 0.83 h / 90 °C

3.1: aluminum (III) chloride / carbon disulfide / 1.5 h / Reflux

4.1: aluminum (III) chloride / 1,2-dichloro-ethane / 5 h / Inert atmosphere; Reflux

4.2: Cooling with ice

5.1: triethylamine / dichloromethane / 2 h / 0 °C / Inert atmosphere

6.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 80 °C / Inert atmosphere

7.1: bromine; acetic acid / chloroform / 70 °C

With Lawessons reagent; aluminum (III) chloride; bromine; sodium carbonate; acetic acid; triethylamine; sodium hydroxide; potassium hexacyanoferrate(III); aluminum (III) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In carbon disulfide; ethanol; dichloromethane; chloroform; water; 1,2-dichloro-ethane; toluene; 6.1: Suzuki Coupling;