tert-butyl (Z,3S,R(S))-[5-methyl-1-(p-tolylsulfinyl)hex-1-en-3-yl]carbamate

Base Information

Chemical Name:tert-butyl (Z,3S,R(S))-[5-methyl-1-(p-tolylsulfinyl)hex-1-en-3-yl]carbamate
CAS No.:1105065-53-9
Molecular Formula:C₁₉H₂₉NO₃S
Molecular Weight:351.51
Hs Code.:

Synonyms:tert-butyl (Z,3S,R(S))-[5-methyl-1-(p-tolylsulfinyl)hex-1-en-3-yl]carbamate

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Chemical Property of tert-butyl (Z,3S,R(S))-[5-methyl-1-(p-tolylsulfinyl)hex-1-en-3-yl]carbamate

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Technology Process of tert-butyl (Z,3S,R(S))-[5-methyl-1-(p-tolylsulfinyl)hex-1-en-3-yl]carbamate

There total 1 articles about tert-butyl (Z,3S,R(S))-[5-methyl-1-(p-tolylsulfinyl)hex-1-en-3-yl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58521-45-2
tert-butoxycarbonyl-L-leucinal

: 63268-43-9
(+)-(S)-dimethyl-p-tolylsulfinylmethanephosphonate

: 1105065-53-9
tert-butyl (Z,3S,R(S))-[5-methyl-1-(p-tolylsulfinyl)hex-1-en-3-yl]carbamate

: 1105065-44-8
tert-butyl (E,3S,R(S))-[5-methyl-1-(p-tolylsulfinyl)hex-1-en-3-yl]carbamate

Guidance literature:: (+)-(S)-dimethyl-p-tolylsulfinylmethanephosphonate; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

tert-butoxycarbonyl-L-leucinal; In tetrahydrofuran; hexane; at -78 - 25 ℃; optical yield given as %de; Inert atmosphere;
DOI:10.1016/j.tet.2008.10.037

Reference yield: 45.0%

: 1105065-53-9
tert-butyl (Z,3S,R(S))-[5-methyl-1-(p-tolylsulfinyl)hex-1-en-3-yl]carbamate

: 5804-85-3
diethylaluminium cyanide

: 1105065-64-2
tert-butyl (2R,3S,R(S))-[2-cyano-5-methyl-1-(p-tolylsulfinyl)hexan-3-yl]carbamate

Guidance literature:: tert-butyl (Z,3S,R(S))-[5-methyl-1-(p-tolylsulfinyl)hex-1-en-3-yl]carbamate; diethylaluminium cyanide; In tetrahydrofuran; toluene; at 0 - 25 ℃; Inert atmosphere;

With rochelle salt; In tetrahydrofuran; toluene; diastereoselective reaction;
DOI:10.1016/j.tet.2008.10.037