(R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (S)-1-methoxycarbonyl-2-phenylsulfanyl-ethyl ester

Base Information

Chemical Name:(R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (S)-1-methoxycarbonyl-2-phenylsulfanyl-ethyl ester
CAS No.:82971-70-8
Molecular Formula:C₂₀H₁₉F₃O₅S
Molecular Weight:428.429
Hs Code.:

Synonyms:(R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (S)-1-methoxycarbonyl-2-phenylsulfanyl-ethyl ester

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Chemical Property of (R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (S)-1-methoxycarbonyl-2-phenylsulfanyl-ethyl ester

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Technology Process of (R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (S)-1-methoxycarbonyl-2-phenylsulfanyl-ethyl ester

There total 10 articles about (R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (S)-1-methoxycarbonyl-2-phenylsulfanyl-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 83023-80-7
(2S)-hydroxy-3-(phenylthio)propanoic acid

: 82971-70-8
(R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (S)-1-methoxycarbonyl-2-phenylsulfanyl-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / diethyl ether / 0.5 h / 25 °C

2: DMAP / CH₂Cl₂

With dmap; In diethyl ether; dichloromethane;
DOI:10.1021/jo00038a028

Reference yield:

: 108-98-5
thiophenol

: 82971-70-8
(R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (S)-1-methoxycarbonyl-2-phenylsulfanyl-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 2.) aq. HCl / 1) methanol, room temperature, 48 h

2: acetyl chloride / 2 h / Heating

3: pyridine / CCl₄ / 8 h

With pyridine; hydrogenchloride; acetyl chloride; In tetrachloromethane;
DOI:10.1021/ja00380a021

Reference yield:

: 83023-80-7,83023-81-8,82971-73-1
2-hydroxy-3-(phenylthio)propionic acid

: 82971-70-8
(R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (S)-1-methoxycarbonyl-2-phenylsulfanyl-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: acetyl chloride / 2 h / Heating

2: pyridine / CCl₄ / 8 h

With pyridine; acetyl chloride; In tetrachloromethane;
DOI:10.1021/ja00380a021