N-[[4-[(1,3-dioxoisoindolin-2-yl)methyl]phenyl]-methyl-oxo-λ⁶-sulfanylidene]-2,2,2-trifluoro-acetamide

Base Information

• Chemical Name: N-[[4-[(1,3-dioxoisoindolin-2-yl)methyl]phenyl]-methyl-oxo-λ⁶-sulfanylidene]-2,2,2-trifluoro-acetamide
• CAS No.: 1570084-40-0
• Molecular Formula: C₁₈H₁₃F₃N₂O₄S
• Molecular Weight: 410.373

Synonyms:N-[[4-[(1,3-dioxoisoindolin-2-yl)methyl]phenyl]-methyl-oxo-λ⁶-sulfanylidene]-2,2,2-trifluoro-acetamide

Chemical Property of N-[[4-[(1,3-dioxoisoindolin-2-yl)methyl]phenyl]-methyl-oxo-λ⁶-sulfanylidene]-2,2,2-trifluoro-acetamide

Chemical Property:

Purity/Quality:

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Technology Process of N-[[4-[(1,3-dioxoisoindolin-2-yl)methyl]phenyl]-methyl-oxo-λ⁶-sulfanylidene]-2,2,2-trifluoro-acetamide

There total 5 articles about N-[[4-[(1,3-dioxoisoindolin-2-yl)methyl]phenyl]-methyl-oxo-λ⁶-sulfanylidene]-2,2,2-trifluoro-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

[[4-[(1,3-dioxoisoindolin-2-yl)methyl]phenyl]-methyl-oxo-λ6-sulfanylidene]cyanamide (1570082-23-3) + trifluoroacetic anhydride (407-25-0) → N-[[4-[(1,3-dioxoisoindolin-2-yl)methyl]phenyl]-methyl-oxo-λ6-sulfanylidene]-2,2,2-trifluoro-acetamide (1570084-40-0)

Guidance literature:

In dichloromethane; at 0 - 20 ℃; for 2h;

Reference yield:

2-(4-methylthiobenzyl)isoindol-1,3-dione (247569-44-4) → N-[[4-[(1,3-dioxoisoindolin-2-yl)methyl]phenyl]-methyl-oxo-λ6-sulfanylidene]-2,2,2-trifluoro-acetamide (1570084-40-0)

Guidance literature:

Multi-step reaction with 3 steps

1: N-Bromosuccinimide; potassium tert-butylate / methanol / 1 h

2: potassium carbonate; 3-chloro-benzenecarboperoxoic acid / ethanol / 0 - 20 °C

3: dichloromethane / 2 h / 0 - 20 °C

With N-Bromosuccinimide; potassium tert-butylate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In methanol; ethanol; dichloromethane;

Reference yield:

4-(methylthio)benzylamine (83171-39-5) → N-[[4-[(1,3-dioxoisoindolin-2-yl)methyl]phenyl]-methyl-oxo-λ6-sulfanylidene]-2,2,2-trifluoro-acetamide (1570084-40-0)

Guidance literature:

Multi-step reaction with 4 steps

1: acetic acid / 3 h / Reflux

2: N-Bromosuccinimide; potassium tert-butylate / methanol / 1 h

3: potassium carbonate; 3-chloro-benzenecarboperoxoic acid / ethanol / 0 - 20 °C

4: dichloromethane / 2 h / 0 - 20 °C

With N-Bromosuccinimide; potassium tert-butylate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In methanol; ethanol; dichloromethane; acetic acid;

upstream raw materials:

[[4-[(1,3-dioxoisoindolin-2-yl)methyl]phenyl]-methyl-oxo-λ⁶-sulfanylidene]cyanamide

trifluoroacetic anhydride

4-(methylthio)benzylamine

phthalic anhydride

Downstream raw materials:

1-isopropyl-6-methyl-4-oxo-5-(3-(trifluoromethyl)phenyl)-1,4-dihydropyridine-3-carboxylic acid 4-(N,S-dimethylsulfonimidoyl)benzylamide

(4-(S-methyl-N-(methylsulfonyl)sulfonimidoyl)phenyl)methanamine

4-(N,S-dimethylsulfonimidoyl)benzylamine

2-(4-(N,S-dimethylsulfonimidoyl)benzyl)isoindoline-1,3-dione

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