N-[(2-bromopyridin-4-yl)methyl]-N-cyclobutyl-1-methyl-1H-imidazole-4-carboxamide

Base Information

Chemical Name:N-[(2-bromopyridin-4-yl)methyl]-N-cyclobutyl-1-methyl-1H-imidazole-4-carboxamide
CAS No.:1365812-37-8
Molecular Formula:C₁₅H₁₇BrN₄O
Molecular Weight:349.23
Hs Code.:

Synonyms:N-[(2-bromopyridin-4-yl)methyl]-N-cyclobutyl-1-methyl-1H-imidazole-4-carboxamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[(2-bromopyridin-4-yl)methyl]-N-cyclobutyl-1-methyl-1H-imidazole-4-carboxamide

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Technology Process of N-[(2-bromopyridin-4-yl)methyl]-N-cyclobutyl-1-methyl-1H-imidazole-4-carboxamide

There total 1 articles about N-[(2-bromopyridin-4-yl)methyl]-N-cyclobutyl-1-methyl-1H-imidazole-4-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1365812-57-2
N-[(2-bromopyridin-4-yl)methyl]cyclobutaneamine

: 41716-18-1
1-methylimidazole-4-carboxylic acid

: 1365812-37-8
N-[(2-bromopyridin-4-yl)methyl]-N-cyclobutyl-1-methyl-1H-imidazole-4-carboxamide

Guidance literature:: 1-methylimidazole-4-carboxylic acid; With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 20 ℃; for 0.25h;

N-[(2-bromopyridin-4-yl)methyl]cyclobutaneamine; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 1365812-37-8
N-[(2-bromopyridin-4-yl)methyl]-N-cyclobutyl-1-methyl-1H-imidazole-4-carboxamide

: 139301-27-2
4-trifluoromethoxyphenylboronic acid

: N-cyclobutyl-1-methyl-N-({2-[4-(trifluoromethoxy)phenyl]pyridin-4-yl}methyl)-1H-imidazole-4-carboxamide dihydrochloride

Guidance literature:: N-[(2-bromopyridin-4-yl)methyl]-N-cyclobutyl-1-methyl-1H-imidazole-4-carboxamide; 4-trifluoromethoxyphenylboronic acid; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; In ethanol; water; toluene; at 150 ℃; for 0.5h; Microwave irradiation;

With hydrogenchloride; In water; acetonitrile;

Reference yield:

: 1365812-37-8
N-[(2-bromopyridin-4-yl)methyl]-N-cyclobutyl-1-methyl-1H-imidazole-4-carboxamide

: 247564-72-3
(2,4,5-trifluorophenyl)boronic acid

: N-cyclobutyl-1-methyl-N-{[2-(2,4,5-trifluorophenyl)pyridin-4-yl]methyl}-1H-imidazole-4-carboxamide dihydrochloride

Guidance literature:: N-[(2-bromopyridin-4-yl)methyl]-N-cyclobutyl-1-methyl-1H-imidazole-4-carboxamide; (2,4,5-trifluorophenyl)boronic acid; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; In ethanol; ethyl acetate; toluene; at 100 ℃; for 3h;

With hydrogenchloride; In water; acetonitrile;