4-Chlormethyl-3-(3-trifluormethylphenyl)-2,3-dihydro-1,3-thiazol-2-thion

Base Information

Chemical Name:4-Chlormethyl-3-(3-trifluormethylphenyl)-2,3-dihydro-1,3-thiazol-2-thion
CAS No.:286374-52-5
Molecular Formula:C₁₁H₇ClF₃NS₂
Molecular Weight:309.763
Hs Code.:

Synonyms:4-Chlormethyl-3-(3-trifluormethylphenyl)-2,3-dihydro-1,3-thiazol-2-thion

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Chemical Property of 4-Chlormethyl-3-(3-trifluormethylphenyl)-2,3-dihydro-1,3-thiazol-2-thion

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Technology Process of 4-Chlormethyl-3-(3-trifluormethylphenyl)-2,3-dihydro-1,3-thiazol-2-thion

There total 3 articles about 4-Chlormethyl-3-(3-trifluormethylphenyl)-2,3-dihydro-1,3-thiazol-2-thion which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 286374-46-7
4-Chlormethyl-4-hydroxy-3-(3-trifluormethylphenyl)-1,3-thiazolidin-2-thion

: 286374-52-5
4-Chlormethyl-3-(3-trifluormethylphenyl)-2,3-dihydro-1,3-thiazol-2-thion

Guidance literature:: With hydrogenchloride; In ethyl acetate; for 2h; Heating;

Reference yield:

: 98-16-8
3-trifluoromethylaniline

: 286374-52-5
4-Chlormethyl-3-(3-trifluormethylphenyl)-2,3-dihydro-1,3-thiazol-2-thion

Guidance literature:: Multi-step reaction with 3 steps

1: 30.12 g / 20 °C

2: 80 percent / methanol; acetone / 2 h / 20 °C

3: 22.08 g / HCl / ethyl acetate / 2 h / Heating

With hydrogenchloride; In methanol; ethyl acetate; acetone; 1: Addition / 2: Cyclization / 3: Dehydration;

Reference yield:

: 3-trifluorophenyl dithiocarbamic acid triethylammonium

: 286374-52-5
4-Chlormethyl-3-(3-trifluormethylphenyl)-2,3-dihydro-1,3-thiazol-2-thion

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / methanol; acetone / 2 h / 20 °C

2: 22.08 g / HCl / ethyl acetate / 2 h / Heating

With hydrogenchloride; In methanol; ethyl acetate; acetone; 1: Cyclization / 2: Dehydration;