N²-(tert-butoxycarbonyl)-N³-(benzyloxycarbonyl)-L-(2,3-diaminopropanoyl)-L-alanine tert-butyl ester

Base Information

• Chemical Name: N²-(tert-butoxycarbonyl)-N³-(benzyloxycarbonyl)-L-(2,3-diaminopropanoyl)-L-alanine tert-butyl ester
• CAS No.: 122593-28-6
• Molecular Formula: C₂₃H₃₅N₃O₇
• Molecular Weight: 465.547

Synonyms:N²-(tert-butoxycarbonyl)-N³-(benzyloxycarbonyl)-L-(2,3-diaminopropanoyl)-L-alanine tert-butyl ester

Chemical Property of N²-(tert-butoxycarbonyl)-N³-(benzyloxycarbonyl)-L-(2,3-diaminopropanoyl)-L-alanine tert-butyl ester

Chemical Property:

Purity/Quality:

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Technology Process of N²-(tert-butoxycarbonyl)-N³-(benzyloxycarbonyl)-L-(2,3-diaminopropanoyl)-L-alanine tert-butyl ester

There total 1 articles about N²-(tert-butoxycarbonyl)-N³-(benzyloxycarbonyl)-L-(2,3-diaminopropanoyl)-L-alanine tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

Ala-OtBu (21691-50-9) + N2-(tert-butoxycarbonyl)-N3-(benzyloxycarbonyl)-L-2,3-diaminopropanoic acid (65710-57-8,81306-93-6) → N2-(tert-butoxycarbonyl)-N3-(benzyloxycarbonyl)-L-(2,3-diaminopropanoyl)-L-alanine tert-butyl ester (122593-28-6)

Guidance literature:

With diphenyl-phosphinic acid; triethylamine; In N,N-dimethyl-formamide; for 12h; Ambient temperature;

DOI:10.1021/jm00163a022

Reference yield: 82.0%

N2-(tert-butoxycarbonyl)-N3-(benzyloxycarbonyl)-L-(2,3-diaminopropanoyl)-L-alanine tert-butyl ester (122593-28-6) + trifluoroacetic acid (76-05-1) → N3-(benzyloxycarbonyl)-L-(2,3-diaminopropanoyl)-L-alanine trifluoroacetate salt (122593-32-2)

Guidance literature:

for 2h; Ambient temperature;

DOI:10.1021/jm00163a022

upstream raw materials:

Ala-OtBu

N²-(tert-butoxycarbonyl)-N³-(benzyloxycarbonyl)-L-2,3-diaminopropanoic acid

Downstream raw materials:

N³-(benzyloxycarbonyl)-L-(2,3-diaminopropanoyl)-L-alanine trifluoroacetate salt

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