C₁₇H₁₄FN₅O₃

Base Information

Chemical Name:C₁₇H₁₄FN₅O₃
CAS No.:1338091-35-2
Molecular Formula:C₁₇H₁₄FN₅O₃
Molecular Weight:355.328
Hs Code.:

C<sub>17</sub>H<sub>14</sub>FN<sub>5</sub>O<sub>3</sub>

Synonyms:C₁₇H₁₄FN₅O₃

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Chemical Property of C₁₇H₁₄FN₅O₃

Chemical Property:

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Technology Process of C₁₇H₁₄FN₅O₃

There total 10 articles about C₁₇H₁₄FN₅O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1338091-34-1
1-methyl-4-oxo-1,4-dihydropyrido[3,2-c]pyridazine-3-carboxylic acid

: 34547-28-9
4-fluorophenylacetic acid hydrazide

: 1338091-35-2
C₁₇H₁₄FN₅O₃

Guidance literature:: With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; In dimethyl sulfoxide; at 20 ℃; for 16h;

Reference yield:

: 405-50-5
p-Fluorophenylacetic acid

: 1338091-35-2
C₁₇H₁₄FN₅O₃

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 1 h / 80 °C

2: hydrazine hydrate / dichloromethane / 1.5 h / 0 - 20 °C

3: triethylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dimethyl sulfoxide / 16 h / 20 °C

With thionyl chloride; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; hydrazine hydrate; triethylamine; In dichloromethane; dimethyl sulfoxide;

Reference yield:

: lithium 3-fluoropyridine-2-carboxylate

: 1338091-35-2
C₁₇H₁₄FN₅O₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: sulfuric acid / 20 h / Reflux

2.1: lithium diisopropyl amide / n-heptane; tetrahydrofuran / 0.75 h / -78 °C

2.2: 2 h / -78 °C

3.1: triethylamine; 4-acetamidobenzenesulfonyl azide / acetonitrile / 0 - 20 °C

4.1: trimethylphosphane / tetrahydrofuran / 20 °C

4.2: 0.25 h / 20 °C

5.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 18 h / 20 °C

6.1: trifluoroacetic acid / dichloromethane / 16 h / 20 °C

7.1: triethylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dimethyl sulfoxide / 16 h / 20 °C

With sulfuric acid; 4-acetamidobenzenesulfonyl azide; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; trifluoroacetic acid; lithium diisopropyl amide; trimethylphosphane; In tetrahydrofuran; n-heptane; dichloromethane; dimethyl sulfoxide; acetonitrile;