1-((2-chloroquinolin-3-yl)methylene)-4-p-nitrophenylthiosemicarbazide

Base Information

Chemical Name:1-((2-chloroquinolin-3-yl)methylene)-4-p-nitrophenylthiosemicarbazide
CAS No.:1313027-74-5
Molecular Formula:C₁₇H₁₂ClN₅O₂S
Molecular Weight:385.834
Hs Code.:

Synonyms:1-((2-chloroquinolin-3-yl)methylene)-4-p-nitrophenylthiosemicarbazide

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Chemical Property of 1-((2-chloroquinolin-3-yl)methylene)-4-p-nitrophenylthiosemicarbazide

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Technology Process of 1-((2-chloroquinolin-3-yl)methylene)-4-p-nitrophenylthiosemicarbazide

There total 3 articles about 1-((2-chloroquinolin-3-yl)methylene)-4-p-nitrophenylthiosemicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 73568-25-9
2-chloro-3-quinoline carboxaldehyde

: 38985-70-5
4-(4-nitrophenyl)-3-thiosemicarbazide

: 1313027-74-5
1-((2-chloroquinolin-3-yl)methylene)-4-p-nitrophenylthiosemicarbazide

Guidance literature:: 2-chloro-3-quinoline carboxaldehyde; 4-(4-nitrophenyl)-3-thiosemicarbazide; In ethanol;

With acetic acid; In ethanol; at 60 ℃; for 12h;
DOI:10.1016/j.ejmech.2011.04.013

Reference yield:

: 13037-51-9
-essigsaeure

: 1313027-74-5
1-((2-chloroquinolin-3-yl)methylene)-4-p-nitrophenylthiosemicarbazide

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrazine hydrate

2.1: ethanol

2.2: 12 h / 60 °C

With hydrazine hydrate; In ethanol;
DOI:10.1016/j.ejmech.2011.04.013

Reference yield:

: 100-01-6,104810-17-5
4-nitro-aniline

: 1313027-74-5
1-((2-chloroquinolin-3-yl)methylene)-4-p-nitrophenylthiosemicarbazide

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hydroxide / water

2.1: hydrazine hydrate

3.1: ethanol

3.2: 12 h / 60 °C

With hydrazine hydrate; potassium hydroxide; In ethanol; water;
DOI:10.1016/j.ejmech.2011.04.013