(23S)-3-O-tert-butyldimethylsilyl-1-detigloyl-11,20-O,O-dibenzyl-22,23-dihydro-23-methoxy-7-oxoazadirachtin

Base Information

Chemical Name:(23S)-3-O-tert-butyldimethylsilyl-1-detigloyl-11,20-O,O-dibenzyl-22,23-dihydro-23-methoxy-7-oxoazadirachtin
CAS No.:959922-43-1
Molecular Formula:C₄₉H₆₄O₁₅Si
Molecular Weight:921.124
Hs Code.:

Synonyms:(23S)-3-O-tert-butyldimethylsilyl-1-detigloyl-11,20-O,O-dibenzyl-22,23-dihydro-23-methoxy-7-oxoazadirachtin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (23S)-3-O-tert-butyldimethylsilyl-1-detigloyl-11,20-O,O-dibenzyl-22,23-dihydro-23-methoxy-7-oxoazadirachtin

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Technology Process of (23S)-3-O-tert-butyldimethylsilyl-1-detigloyl-11,20-O,O-dibenzyl-22,23-dihydro-23-methoxy-7-oxoazadirachtin

There total 3 articles about (23S)-3-O-tert-butyldimethylsilyl-1-detigloyl-11,20-O,O-dibenzyl-22,23-dihydro-23-methoxy-7-oxoazadirachtin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 959923-25-2
(23S)-3-desacetyl-1-detigloyl-11,20-bis-O-benzyl-22,23-dihydro-23-methoxy-7-oxoazadirachtin

: 69739-34-0
t-butyldimethylsiyl triflate

: 959922-43-1
(23S)-3-O-tert-butyldimethylsilyl-1-detigloyl-11,20-O,O-dibenzyl-22,23-dihydro-23-methoxy-7-oxoazadirachtin

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at -78 ℃;
DOI:10.1002/anie.200703028

Reference yield: 65.0%

: 1009630-04-9
(23S)-3-O-tert-butyldimethylsilyl-13,14-desepoxy-1-detigloyl-11,20-O,O-dibenzyl-22,23-dihydro-23-methoxy-7-oxoazadirachtin

: 959922-43-1
(23S)-3-O-tert-butyldimethylsilyl-1-detigloyl-11,20-O,O-dibenzyl-22,23-dihydro-23-methoxy-7-oxoazadirachtin

Guidance literature:: With Santonox R; sodium hydrogencarbonate; magnesium monoperoxyphthalate hexahydrate; In methanol; at 110 ℃; for 168h;
DOI:10.1002/chem.200801103

Reference yield: 22.0%

: 1109213-30-0
(23R)-3-O-tert-butyldimethylsilyl-13,14-desepoxy-1-detigloyl-11,20-O,O-dibenzyl-22,23-dihydro-23-methoxy-7-oxoazadirachtin

: 959922-43-1
(23S)-3-O-tert-butyldimethylsilyl-1-detigloyl-11,20-O,O-dibenzyl-22,23-dihydro-23-methoxy-7-oxoazadirachtin

Guidance literature:: With Santonox R; sodium hydrogencarbonate; magnesium monoperoxyphthalate hexahydrate; In methanol; at 110 ℃; for 168h;
DOI:10.1002/chem.200801103