3-((3S,7R,8R,9αR)-2-benzyl-7,8-dimethyl-3-phenyl-octahydro-1H-pyrido[1,2-α]pyrazin-8-yl)benzamide

Base Information

• Chemical Name: 3-((3S,7R,8R,9αR)-2-benzyl-7,8-dimethyl-3-phenyl-octahydro-1H-pyrido[1,2-α]pyrazin-8-yl)benzamide
• CAS No.: 918829-10-4
• Molecular Formula: C₃₀H₃₅N₃O
• Molecular Weight: 453.627

Synonyms:3-((3S,7R,8R,9αR)-2-benzyl-7,8-dimethyl-3-phenyl-octahydro-1H-pyrido[1,2-α]pyrazin-8-yl)benzamide

Chemical Property of 3-((3S,7R,8R,9αR)-2-benzyl-7,8-dimethyl-3-phenyl-octahydro-1H-pyrido[1,2-α]pyrazin-8-yl)benzamide

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Technology Process of 3-((3S,7R,8R,9αR)-2-benzyl-7,8-dimethyl-3-phenyl-octahydro-1H-pyrido[1,2-α]pyrazin-8-yl)benzamide

There total 2 articles about 3-((3S,7R,8R,9αR)-2-benzyl-7,8-dimethyl-3-phenyl-octahydro-1H-pyrido[1,2-α]pyrazin-8-yl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

3-(2-benzyl-7,8-dimethyl-3-phenyl-octahydro-pyrido[1,2-a]pyrazin-8-yl)-benzoic acid (918931-71-2) → 3-((3S,7R,8R,9αR)-2-benzyl-7,8-dimethyl-3-phenyl-octahydro-1H-pyrido[1,2-α]pyrazin-8-yl)benzamide (918829-10-4)

Guidance literature:

With ammonium chloride; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 4h;

Reference yield: 91.0%

3-((3S,7R,8R,9aR)-2-benzyl-7,8-dimethyl-3-phenyl-octahydro-1H-pyrido[1,2-a]pyrazin-8-yl)benzoic acid dihydrochloride → 3-((3S,7R,8R,9αR)-2-benzyl-7,8-dimethyl-3-phenyl-octahydro-1H-pyrido[1,2-α]pyrazin-8-yl)benzamide (918829-10-4)

Guidance literature:

With ammonium chloride; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 4h;

DOI:10.1021/jm0604878

Reference yield: 12.0%

3-((3S,7R,8R,9αR)-2-benzyl-7,8-dimethyl-3-phenyl-octahydro-1H-pyrido[1,2-α]pyrazin-8-yl)benzamide (918829-10-4) → 3-((3S,7R,8R,9αR)-7,8-dimethyl-3-phenyl-octahydro-1H-pyrido[1,2-α]pyrazin-8-yl)benzamide

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; at 20 ℃; for 16h;

DOI:10.1021/jm0604878

upstream raw materials:

3-(2-benzyl-7,8-dimethyl-3-phenyl-octahydro-pyrido[1,2-a]pyrazin-8-yl)-benzoic acid

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