C₂₂H₂₇N₃O₅

Base Information

Chemical Name:C₂₂H₂₇N₃O₅
CAS No.:1253217-74-1
Molecular Formula:C₂₂H₂₇N₃O₅
Molecular Weight:413.473
Hs Code.:

C<sub>22</sub>H<sub>27</sub>N<sub>3</sub>O<sub>5</sub>

Synonyms:C₂₂H₂₇N₃O₅

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Chemical Property of C₂₂H₂₇N₃O₅

Chemical Property:

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Technology Process of C₂₂H₂₇N₃O₅

There total 8 articles about C₂₂H₂₇N₃O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 939430-71-4
6-chloro-5-methoxymethoxy-pyridine-2-carbaldehyde

: 1253217-74-1
C₂₂H₂₇N₃O₅

Guidance literature:: Multi-step reaction with 8 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

1.2: 2.83 h / -78 - 20 °C

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate / 1,2-dimethoxyethane; water / 11 h / 90 °C / Inert atmosphere

3.1: pyridine / 6.5 h

4.1: palladium 10% on activated carbon; hydrogen / acetic acid; ethyl acetate / 14 h

5.1: acetic acid / ethanol / 15 h / 20 - 50 °C

6.1: caesium carbonate / acetonitrile / 4 h / 20 °C

7.1: hydroxylamine hydrochloride; sodium hydrogencarbonate / methanol / 1.5 h / Reflux

8.1: 1,4-dioxane / 4 h / Reflux

With pyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; palladium 10% on activated carbon; hydroxylamine hydrochloride; hydrogen; sodium hydrogencarbonate; caesium carbonate; acetic acid; In tetrahydrofuran; 1,4-dioxane; methanol; 1,2-dimethoxyethane; ethanol; hexane; water; acetic acid; ethyl acetate; acetonitrile;

Reference yield:

: 848442-41-1
C₁₂H₁₇BrO₂

: 1253217-74-1
C₂₂H₂₇N₃O₅

Guidance literature:: Multi-step reaction with 8 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

1.2: 2.83 h / -78 - 20 °C

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate / 1,2-dimethoxyethane; water / 11 h / 90 °C / Inert atmosphere

3.1: pyridine / 6.5 h

4.1: palladium 10% on activated carbon; hydrogen / acetic acid; ethyl acetate / 14 h

5.1: acetic acid / ethanol / 15 h / 20 - 50 °C

6.1: caesium carbonate / acetonitrile / 4 h / 20 °C

7.1: hydroxylamine hydrochloride; sodium hydrogencarbonate / methanol / 1.5 h / Reflux

8.1: 1,4-dioxane / 4 h / Reflux

With pyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; palladium 10% on activated carbon; hydroxylamine hydrochloride; hydrogen; sodium hydrogencarbonate; caesium carbonate; acetic acid; In tetrahydrofuran; 1,4-dioxane; methanol; 1,2-dimethoxyethane; ethanol; hexane; water; acetic acid; ethyl acetate; acetonitrile;

Reference yield:

: 1253214-82-2
C₂₀H₂₆ClNO₅

: 1253217-74-1
C₂₂H₂₇N₃O₅

Guidance literature:: Multi-step reaction with 7 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate / 1,2-dimethoxyethane; water / 11 h / 90 °C / Inert atmosphere

2: pyridine / 6.5 h

3: palladium 10% on activated carbon; hydrogen / acetic acid; ethyl acetate / 14 h

4: acetic acid / ethanol / 15 h / 20 - 50 °C

5: caesium carbonate / acetonitrile / 4 h / 20 °C

6: hydroxylamine hydrochloride; sodium hydrogencarbonate / methanol / 1.5 h / Reflux

7: 1,4-dioxane / 4 h / Reflux

With pyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; hydroxylamine hydrochloride; hydrogen; sodium hydrogencarbonate; caesium carbonate; acetic acid; In 1,4-dioxane; methanol; 1,2-dimethoxyethane; ethanol; water; acetic acid; ethyl acetate; acetonitrile;