Technology Process of 12-(4-iodophenylethynyl)-5,10,15,20-tetraphenyl-21H,23H-porphinatozinc(II)
There total 3 articles about 12-(4-iodophenylethynyl)-5,10,15,20-tetraphenyl-21H,23H-porphinatozinc(II) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
zinc diacetate;
In
methanol; chloroform;
at 20 ℃;
for 1h;
DOI:10.1002/chem.201003200
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrabutylammomium bromide; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 20 °C / Inert atmosphere
2: potassium tert-butylate / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere
3: zinc diacetate / methanol; chloroform / 1 h / 20 °C
With
potassium tert-butylate; zinc diacetate; tetrabutylammomium bromide; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
tetrahydrofuran; methanol; dichloromethane; chloroform;
DOI:10.1002/chem.201003200
- Guidance literature:
-
Multi-step reaction with 4 steps
1: magnesium oxide / 20 °C
2: tetrabutylammomium bromide; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 20 °C / Inert atmosphere
3: potassium tert-butylate / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere
4: zinc diacetate / methanol; chloroform / 1 h / 20 °C
With
potassium tert-butylate; zinc diacetate; tetrabutylammomium bromide; magnesium oxide; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
tetrahydrofuran; methanol; dichloromethane; chloroform;
DOI:10.1002/chem.201003200
