Tyr-Pro-Phe

Base Information

• Chemical Name: Tyr-Pro-Phe
• CAS No.: 72122-59-9
• Molecular Formula: C23H27 N3 O5
• Molecular Weight: 425.48
• DSSTox Substance ID: DTXSID30405408
• Mol file: 72122-59-9.mol

Synonyms:Tyr-Pro-Phe;72122-59-9;BETA-CASOMORPHIN (1-3);tyrosylprolylphenylalanine;2-[[1-[2-amino-3-(4-hydroxyphenyl)propanoyl]pyrrolidine-2-carbonyl]amino]-3-phenylpropanoic acid;beta-Casomorphin-3;BETA-CASOMORPHIN(1-3);b-Casomorphin (1-3);DTXSID30405408;RCMWNNJFKNDKQR-UHFFFAOYSA-N;FT-0641392;YPF

Chemical Property of Tyr-Pro-Phe

Chemical Property:

• Storage Temp.: -15°C
• XLogP3: -0.7
• Hydrogen Bond Donor Count: 4
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 8
• Exact Mass: 425.19507097
• Heavy Atom Count: 31
• Complexity: 629

Purity/Quality:

99%, ^*data from raw suppliers

Beta-Casomorphin (1-3) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CC(N(C1)C(=O)C(CC2=CC=C(C=C2)O)N)C(=O)NC(CC3=CC=CC=C3)C(=O)O

Technology Process of Tyr-Pro-Phe

There total 5 articles about Tyr-Pro-Phe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

Z-Tyr(OBzl)-Pro-Phe-OH (92278-85-8) → β-Casomorphin 3 (72122-59-9)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol;

DOI:10.1007/s10600-006-0079-5

Reference yield:

Z-Tyr(OBzl)-Pro-ONSu → β-Casomorphin 3 (72122-59-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.23 g / aq. NaOH / dimethylformamide

2: 76 percent / H₂ / Pd/C / methanol

With sodium hydroxide; hydrogen; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;

DOI:10.1007/s10600-006-0079-5

Reference yield:

Z-Tyr(OBzl)-ONp (3562-03-6) → β-Casomorphin 3 (72122-59-9)

Guidance literature:

Multi-step reaction with 4 steps

1: 72 percent / aq. NaOH / dimethylformamide

2: DCC / ethyl acetate

3: 1.23 g / aq. NaOH / dimethylformamide

4: 76 percent / H₂ / Pd/C / methanol

With sodium hydroxide; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; ethyl acetate; N,N-dimethyl-formamide;

DOI:10.1007/s10600-006-0079-5

upstream raw materials:

Z-Tyr(OBzl)-Pro-Phe-OH

Z-Tyr(OBzl)-ONp

Z-Tyr(OBzl)-Pro-OH

L-proline

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