alpha-D-Ribofuranoside,methyl2-amino-3-carboxy-2,3,5-trideoxy-(9CI)

Base Information

Chemical Name:alpha-D-Ribofuranoside,methyl2-amino-3-carboxy-2,3,5-trideoxy-(9CI)
CAS No.:755742-83-7
Molecular Formula:C₇H₁₃NO₄
Molecular Weight:175.185
Hs Code.:
Mol file:755742-83-7.mol

Synonyms:alpha-D-Ribofuranoside,methyl2-amino-3-carboxy-2,3,5-trideoxy-(9CI)

Suppliers and Price of alpha-D-Ribofuranoside,methyl2-amino-3-carboxy-2,3,5-trideoxy-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of alpha-D-Ribofuranoside,methyl2-amino-3-carboxy-2,3,5-trideoxy-(9CI)

Chemical Property:

PSA：81.78000
LogP:0.10600

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of alpha-D-Ribofuranoside,methyl2-amino-3-carboxy-2,3,5-trideoxy-(9CI)

There total 4 articles about alpha-D-Ribofuranoside,methyl2-amino-3-carboxy-2,3,5-trideoxy-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: Sodium; 2-((2S,3R,4S,5R)-4-carboxy-2-methoxy-5-methyl-tetrahydro-furan-3-ylsulfamoyl)-benzenesulfonate

: 755742-83-7
(2R,3S,4R,5S)-4-Amino-5-methoxy-2-methyl-tetrahydro-furan-3-carboxylic acid

Guidance literature:: With ammonia; lithium; sodium hydrogencarbonate; In methanol; at -40 ℃; for 1h;
DOI:10.7164/antibiotics.53.1231

Reference yield:

: methyl 2-amino-2,6-dideoxy-α-D-glucopyranoside

: 755742-83-7
(2R,3S,4R,5S)-4-Amino-5-methoxy-2-methyl-tetrahydro-furan-3-carboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / pyridine / 2 h / 20 °C

2: potassium tert-butoxide / tetrahydrofuran / 1 h / 0 °C

3: HOSO₂NH₂; NaClO₂ / dioxane; H₂O / 0.5 h / 20 °C

4: 92 percent / NaHCO₃; Li/liq. NH₃ / methanol / 1 h / -40 °C

With pyridine; sodium chlorite; amidosulfuric acid fluoride; potassium tert-butylate; ammonia; lithium; sodium hydrogencarbonate; In tetrahydrofuran; 1,4-dioxane; methanol; water; 4: Birch reduction;
DOI:10.7164/antibiotics.53.1231

Reference yield:

: 313986-20-8
1-methoxy-3-methyl-6,6,11,11-tetraoxo-4,4a,6,11,12,12a-hexahydro-1H,3H-2,5-dioxa-6λ⁶,11λ⁶-dithia-12-aza-dibenzo[a,e]cycloocten-4-ol

: 755742-83-7
(2R,3S,4R,5S)-4-Amino-5-methoxy-2-methyl-tetrahydro-furan-3-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: potassium tert-butoxide / tetrahydrofuran / 1 h / 0 °C

2: HOSO₂NH₂; NaClO₂ / dioxane; H₂O / 0.5 h / 20 °C

3: 92 percent / NaHCO₃; Li/liq. NH₃ / methanol / 1 h / -40 °C

With sodium chlorite; amidosulfuric acid fluoride; potassium tert-butylate; ammonia; lithium; sodium hydrogencarbonate; In tetrahydrofuran; 1,4-dioxane; methanol; water; 3: Birch reduction;
DOI:10.7164/antibiotics.53.1231