C₃⁽¹³⁾C₃H₄⁽²⁾H₃⁽¹⁵⁾N

Base Information

• Chemical Name: C₃⁽¹³⁾C₃H₄⁽²⁾H₃⁽¹⁵⁾N
• CAS No.: 851476-59-0
• Molecular Formula: C₆H₇N
• Molecular Weight: 100.065
• Mol file: 851476-59-0.mol

Synonyms:C₃⁽¹³⁾C₃H₄⁽²⁾H₃⁽¹⁵⁾N

Chemical Property of C₃⁽¹³⁾C₃H₄⁽²⁾H₃⁽¹⁵⁾N

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃⁽¹³⁾C₃H₄⁽²⁾H₃⁽¹⁵⁾N

There total 7 articles about C₃⁽¹³⁾C₃H₄⁽²⁾H₃⁽¹⁵⁾N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C3(13)C3H6(2)H(15)N*ClH → C3(13)C3H4(2)H3(15)N (851476-59-0)

Guidance literature:

C₃⁽¹³⁾C₃H₆⁽²⁾H⁽¹⁵⁾N*ClH; With water-d2; at 120 ℃; for 48h;

With sodium hydroxide; In water; at 0 ℃;

Reference yield:

C13(13)C3H12(2)H2N4O3 → C3(13)C3H4(2)H3(15)N (851476-59-0)

Guidance literature:

Multi-step reaction with 5 steps

1: palladium on activated charcoal; sodium carbonate; deuterium / benzene

2: methanol; sodium hydroxide

3: thionyl chloride

4: <15N>ammonium acetate / acetone

5: sodium hypochlorite solution / Heating

With methanol; thionyl chloride; sodium hypochlorite solution; palladium on activated charcoal; sodium carbonate; <15N>ammonium acetate; deuterium; sodium hydroxide; In acetone; benzene; 5: Hofmann rearrangement;

DOI:10.1007/s10858-011-9568-3

Reference yield:

C4(13)C3H3(2)H3O2 → C3(13)C3H4(2)H3(15)N (851476-59-0)

Guidance literature:

Multi-step reaction with 3 steps

1: thionyl chloride

2: <15N>ammonium acetate / acetone

3: sodium hypochlorite solution / Heating

With thionyl chloride; sodium hypochlorite solution; <15N>ammonium acetate; In acetone; 3: Hofmann rearrangement;

DOI:10.1007/s10858-011-9568-3