N-<(SR,SR)-2,4-bis(cyclohexylmethyl)-4-carboxybutyryl>-β-alanine disodium salt

Base Information

Chemical Name:N-<(SR,SR)-2,4-bis(cyclohexylmethyl)-4-carboxybutyryl>-β-alanine disodium salt
CAS No.:105129-26-8
Molecular Formula:C₂₂H₃₅NO₅*2Na
Molecular Weight:439.503
Hs Code.:

Synonyms:N-<(SR,SR)-2,4-bis(cyclohexylmethyl)-4-carboxybutyryl>-β-alanine disodium salt

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Chemical Property of N-<(SR,SR)-2,4-bis(cyclohexylmethyl)-4-carboxybutyryl>-β-alanine disodium salt

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Technology Process of N-<(SR,SR)-2,4-bis(cyclohexylmethyl)-4-carboxybutyryl>-β-alanine disodium salt

There total 4 articles about N-<(SR,SR)-2,4-bis(cyclohexylmethyl)-4-carboxybutyryl>-β-alanine disodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 105148-48-9
N-<(SR,SR)-2,4-dibenzyl-4-carboxybutyryl>-β-alanine

: 105129-26-8
N-<(SR,SR)-2,4-bis(cyclohexylmethyl)-4-carboxybutyryl>-β-alanine disodium salt

Guidance literature:: With sodium hydroxide; hydrogen; Rh on carbon; 1) EtOH, H₂O, 50 psi, 36 h, 2) MeOH;
DOI:10.1021/jm00132a005

Reference yield:

: 105129-13-3
threo-2,4-dibenzylglutaric acid

: 105129-26-8
N-<(SR,SR)-2,4-bis(cyclohexylmethyl)-4-carboxybutyryl>-β-alanine disodium salt

Guidance literature:: Multi-step reaction with 4 steps

1: acetyl chloride / toluene / 2 h

2: 15percent Et₃N / toluene / 0.25 h / 50 °C

3: 90 percent / pyridine / CH₂Cl₂ / 16 h / Ambient temperature

4: 56 percent / 1) H₂, 2) 1 N NaOH / 1) 5percent Rh/C / 1) EtOH, H₂O, 50 psi, 36 h, 2) MeOH

With pyridine; sodium hydroxide; hydrogen; triethylamine; acetyl chloride; Rh on carbon; In dichloromethane; toluene;
DOI:10.1021/jm00132a005

Reference yield:

: 105129-11-1
cis-2,4-dibenzylglutaric anhydride

: 105129-26-8
N-<(SR,SR)-2,4-bis(cyclohexylmethyl)-4-carboxybutyryl>-β-alanine disodium salt

Guidance literature:: Multi-step reaction with 3 steps

1: 15percent Et₃N / toluene / 0.25 h / 50 °C

2: 90 percent / pyridine / CH₂Cl₂ / 16 h / Ambient temperature

3: 56 percent / 1) H₂, 2) 1 N NaOH / 1) 5percent Rh/C / 1) EtOH, H₂O, 50 psi, 36 h, 2) MeOH

With pyridine; sodium hydroxide; hydrogen; triethylamine; Rh on carbon; In dichloromethane; toluene;
DOI:10.1021/jm00132a005