C₁₄H₂₃O₅P

Base Information

Chemical Name:C₁₄H₂₃O₅P
CAS No.:1574233-51-4
Molecular Formula:C₁₄H₂₃O₅P
Molecular Weight:302.307
Hs Code.:

C<sub>14</sub>H<sub>23</sub>O<sub>5</sub>P

Synonyms:C₁₄H₂₃O₅P

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Chemical Property of C₁₄H₂₃O₅P

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Technology Process of C₁₄H₂₃O₅P

There total 5 articles about C₁₄H₂₃O₅P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.5%

: 1574233-44-5
diethyl (1S,2S)-(1-benzyloxy-2-hydroxy-4-phenylbutyl)phosphonate

: 1574233-51-4
C₁₄H₂₃O₅P

Guidance literature:: With palladium 10% on activated carbon; hydrogen; acetic acid; In ethanol; for 24h;
DOI:10.1021/jo500148j

Reference yield: 86.4%

: 135760-96-2
diethyl (E)-(4-phenylbut-1-en-1-yl)phosphonate

: 1574233-51-4
C₁₄H₂₃O₅P

Guidance literature:: With methanesulfonamide; (DHQD)₂Phal; In water; tert-butyl alcohol; at 0 ℃; for 48h; Inert atmosphere;
DOI:10.1021/jo500148j

Reference yield:

: 89268-01-9
(phenylmethoxy)methylphosphonic acid diethyl ester

: 1574233-51-4
C₁₄H₂₃O₅P

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 0.75 h / -5 - 0 °C / Inert atmosphere

2.1: triethylamine; RuCl[(1R,2R)-p-TsNCH(C6H5)CH-(C6H5)NH2](η6-benzene) / 0.17 h / 20 °C / Inert atmosphere

2.2: 5 h / 35 °C / Inert atmosphere

3.1: acetic acid; palladium 10% on activated carbon; hydrogen / ethanol / 24 h

With RuCl[(1R,2R)-p-TsNCH(C6H5)CH-(C6H5)NH2](η6-benzene); palladium 10% on activated carbon; hydrogen; acetic acid; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; ethanol;
DOI:10.1021/jo500148j