(+)-(E)-1-[4-(5-phenyl-3-(trifluoromethyl)pent-1-en-1yl)phenyl]ethanone

Base Information

Chemical Name:(+)-(E)-1-[4-(5-phenyl-3-(trifluoromethyl)pent-1-en-1yl)phenyl]ethanone
CAS No.:1426582-95-7
Molecular Formula:C₂₀H₁₉F₃O
Molecular Weight:332.365
Hs Code.:

Synonyms:(+)-(E)-1-[4-(5-phenyl-3-(trifluoromethyl)pent-1-en-1yl)phenyl]ethanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+)-(E)-1-[4-(5-phenyl-3-(trifluoromethyl)pent-1-en-1yl)phenyl]ethanone

Chemical Property:

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Technology Process of (+)-(E)-1-[4-(5-phenyl-3-(trifluoromethyl)pent-1-en-1yl)phenyl]ethanone

There total 5 articles about (+)-(E)-1-[4-(5-phenyl-3-(trifluoromethyl)pent-1-en-1yl)phenyl]ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 887144-94-7
Togni's reagent II

: 1426582-68-4
(1R,2E)-1-[4-[5-phenyl-1-(trimethylsilyl)pent-2-en-1yl]phenyl]ethanone

: 1426582-99-1
(+)-(Z)-1-[4-(5-phenyl-3-(trifluoromethyl)pent-1-en-1yl)phenyl]ethanone

: 1426582-95-7
(+)-(E)-1-[4-(5-phenyl-3-(trifluoromethyl)pent-1-en-1yl)phenyl]ethanone

: (E)-1-[4-(5-phenyl-3-(trifluoromethyl)pent-1-en-1yl)phenyl]ethanone

Guidance literature:: With tris(bipyridine)ruthenium(II) dichloride hexahydrate; In methanol; at 20 ℃; Irradiation;
DOI:10.1021/ol400184t

Reference yield:

: 1426582-72-0
(S,E)-5-phenyl-1-(trimethylsilyl)pent-1-en-3-ol

: 1426582-99-1
(+)-(Z)-1-[4-(5-phenyl-3-(trifluoromethyl)pent-1-en-1yl)phenyl]ethanone

: 1426582-95-7
(+)-(E)-1-[4-(5-phenyl-3-(trifluoromethyl)pent-1-en-1yl)phenyl]ethanone

: (E)-1-[4-(5-phenyl-3-(trifluoromethyl)pent-1-en-1yl)phenyl]ethanone

Guidance literature:: Multi-step reaction with 3 steps

1: dmap; pyridine / dichloromethane / 4 h / 0 - 20 °C

2: palladium diacetate; 1,10-Phenanthroline; silver hexafluoroantimonate; p-benzoquinone / 1,2-dichloro-ethane / 18 h / 60 °C

3: tris(bipyridine)ruthenium(II) dichloride hexahydrate / methanol / 20 °C / Irradiation

With pyridine; dmap; silver hexafluoroantimonate; 1,10-Phenanthroline; tris(bipyridine)ruthenium(II) dichloride hexahydrate; palladium diacetate; p-benzoquinone; In methanol; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/ol400184t

Reference yield:

: 1426582-73-1
(3S,1E)-5-phenyl-1-(trimethylsilyl)pent-1-en-3-yl 2-methoxybenzoate

: 1426582-99-1
(+)-(Z)-1-[4-(5-phenyl-3-(trifluoromethyl)pent-1-en-1yl)phenyl]ethanone

: 1426582-95-7
(+)-(E)-1-[4-(5-phenyl-3-(trifluoromethyl)pent-1-en-1yl)phenyl]ethanone

: (E)-1-[4-(5-phenyl-3-(trifluoromethyl)pent-1-en-1yl)phenyl]ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: palladium diacetate; 1,10-Phenanthroline; silver hexafluoroantimonate; p-benzoquinone / 1,2-dichloro-ethane / 18 h / 60 °C

2: tris(bipyridine)ruthenium(II) dichloride hexahydrate / methanol / 20 °C / Irradiation

With silver hexafluoroantimonate; 1,10-Phenanthroline; tris(bipyridine)ruthenium(II) dichloride hexahydrate; palladium diacetate; p-benzoquinone; In methanol; 1,2-dichloro-ethane;
DOI:10.1021/ol400184t