methyl 4-O-methanesulfonylquinate

Base Information

Chemical Name:methyl 4-O-methanesulfonylquinate
CAS No.:901129-91-7
Molecular Formula:C₉H₁₆O₈S
Molecular Weight:284.287
Hs Code.:

Synonyms:methyl 4-O-methanesulfonylquinate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 4-O-methanesulfonylquinate

Chemical Property:

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Technology Process of methyl 4-O-methanesulfonylquinate

There total 4 articles about methyl 4-O-methanesulfonylquinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 901129-88-2
methyl 3,5-di-O-(tert-butyldimethylsilyl)-4-O-methanesulfonylquinate

: 901129-91-7
methyl 4-O-methanesulfonylquinate

Guidance literature:: With hydrogenchloride; In methanol; at 20 ℃; for 4h;
DOI:10.1021/jo0606249

Reference yield:

: 77-95-2
D-(-)-quinic acid

: 901129-91-7
methyl 4-O-methanesulfonylquinate

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / HCl / 6 h / 60 °C

2: 75 percent / Et₃N / dimethylformamide / 18 h / 0 - 20 °C

3: 80 percent / pyridine / 8 h / 20 °C

4: 75 percent / aq. HCl / methanol / 4 h / 20 °C

With pyridine; hydrogenchloride; triethylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jo0606249

Reference yield:

: 191916-39-9
methyl (-)-quinate

: 901129-91-7
methyl 4-O-methanesulfonylquinate

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / Et₃N / dimethylformamide / 18 h / 0 - 20 °C

2: 80 percent / pyridine / 8 h / 20 °C

3: 75 percent / aq. HCl / methanol / 4 h / 20 °C

With pyridine; hydrogenchloride; triethylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jo0606249