(5-chloro-1,2-dihydro-3-iodo-1-methyl-2-oxo-4-pyridinyl)methyl benzoate

Base Information

Chemical Name:(5-chloro-1,2-dihydro-3-iodo-1-methyl-2-oxo-4-pyridinyl)methyl benzoate
CAS No.:1202474-10-9
Molecular Formula:C₁₄H₁₁ClINO₃
Molecular Weight:403.604
Hs Code.:

Synonyms:(5-chloro-1,2-dihydro-3-iodo-1-methyl-2-oxo-4-pyridinyl)methyl benzoate

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Chemical Property of (5-chloro-1,2-dihydro-3-iodo-1-methyl-2-oxo-4-pyridinyl)methyl benzoate

Chemical Property:

Purity/Quality:

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Technology Process of (5-chloro-1,2-dihydro-3-iodo-1-methyl-2-oxo-4-pyridinyl)methyl benzoate

There total 7 articles about (5-chloro-1,2-dihydro-3-iodo-1-methyl-2-oxo-4-pyridinyl)methyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1202474-09-6
(5-chloro-1,2-dihydro-3-iodo-2-oxo-4-pyridinyl)methyl benzoate

: 77-78-1
dimethyl sulfate

: 1202474-10-9
(5-chloro-1,2-dihydro-3-iodo-1-methyl-2-oxo-4-pyridinyl)methyl benzoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 18h;

Reference yield:

: 215437-47-1
5-chloro-2-(phenylmethoxy)pyridine

: 1202474-10-9
(5-chloro-1,2-dihydro-3-iodo-1-methyl-2-oxo-4-pyridinyl)methyl benzoate

Guidance literature:: Multi-step reaction with 6 steps

1.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexanes / -70 - -65 °C

1.2: 0.42 h

1.3: 20 °C

2.1: diisobutylaluminium hydride / dichloromethane; toluene / -78 - 20 °C

2.2: 1 h

3.1: triethylamine / dichloromethane / 16 h / 20 °C

4.1: trifluoroacetic acid / 48 h / 20 °C

5.1: N-iodo-succinimide / N,N-dimethyl-formamide / 3 h / 65 °C

6.1: potassium carbonate / N,N-dimethyl-formamide / 18 h / 20 °C

With N-iodo-succinimide; n-butyllithium; diisobutylaluminium hydride; potassium carbonate; triethylamine; diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; hexanes; dichloromethane; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1202474-06-3
5-chloro-2-(phenylmethoxy)-4-pyridinemethanol

: 1202474-10-9
(5-chloro-1,2-dihydro-3-iodo-1-methyl-2-oxo-4-pyridinyl)methyl benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / dichloromethane / 16 h / 20 °C

2: trifluoroacetic acid / 48 h / 20 °C

3: N-iodo-succinimide / N,N-dimethyl-formamide / 3 h / 65 °C

4: potassium carbonate / N,N-dimethyl-formamide / 18 h / 20 °C

With N-iodo-succinimide; potassium carbonate; triethylamine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;