(S)-2-{1-(1H-benzo[d][1,2,3]triazol-1-yl)-1-oxo-3-phenylpropan-2-ylamino}naphthalene-1,4-dione

Base Information

• Chemical Name: (S)-2-{1-(1H-benzo[d][1,2,3]triazol-1-yl)-1-oxo-3-phenylpropan-2-ylamino}naphthalene-1,4-dione
• CAS No.: 1212279-46-3
• Molecular Formula: C₂₅H₁₈N₄O₃
• Molecular Weight: 422.443

Synonyms:(S)-2-{1-(1H-benzo[d][1,2,3]triazol-1-yl)-1-oxo-3-phenylpropan-2-ylamino}naphthalene-1,4-dione

Chemical Property of (S)-2-{1-(1H-benzo[d][1,2,3]triazol-1-yl)-1-oxo-3-phenylpropan-2-ylamino}naphthalene-1,4-dione

Chemical Property:

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Technology Process of (S)-2-{1-(1H-benzo[d][1,2,3]triazol-1-yl)-1-oxo-3-phenylpropan-2-ylamino}naphthalene-1,4-dione

There total 1 articles about (S)-2-{1-(1H-benzo[d][1,2,3]triazol-1-yl)-1-oxo-3-phenylpropan-2-ylamino}naphthalene-1,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

1,2,3-Benzotriazole (95-14-7,27556-51-0) + (S)-2-(1,4-dioxo-1,4-dihydronaphthalen-2-ylamino)-3-phenylpropanoic acid (1212330-93-2) → (S)-2-{1-(1H-benzo[d][1,2,3]triazol-1-yl)-1-oxo-3-phenylpropan-2-ylamino}naphthalene-1,4-dione (1212279-46-3)

Guidance literature:

With dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 4h;

DOI:10.1055/s-0029-1220012

Reference yield: 81.0%

L-valine (72-18-4,25609-85-2,7004-03-7,921-10-8) + (S)-2-{1-(1H-benzo[d][1,2,3]triazol-1-yl)-1-oxo-3-phenylpropan-2-ylamino}naphthalene-1,4-dione (1212279-46-3) → (S)-2-[(S)-2-(1,4-dioxo-1,4-dihydronaphthalen-2-ylamino)-3-phenylpropanamido]-3-methylbutanoic acid (1242672-19-0)

Guidance literature:

With triethylamine; In water; acetonitrile; at 20 ℃; for 4h;

DOI:10.1055/s-0029-1220012

Reference yield: 81.0%

(S)-2-{1-(1H-benzo[d][1,2,3]triazol-1-yl)-1-oxo-3-phenylpropan-2-ylamino}naphthalene-1,4-dione (1212279-46-3) + L-Tryptophan (73-22-3,27732-43-0,80206-30-0,27813-82-7) → (S)-2-[(S)-2-(1,4-dioxo-1,4-dihydronaphthalen-2-ylamino)-3-phenylpropanamido]-3-(1H-indol-3-yl)propanoic acid (1242672-20-3)

Guidance literature:

With triethylamine; In water; acetonitrile; at 20 ℃; for 4h;

DOI:10.1055/s-0029-1220012

upstream raw materials:

1,2,3-Benzotriazole

(S)-2-(1,4-dioxo-1,4-dihydronaphthalen-2-ylamino)-3-phenylpropanoic acid

Downstream raw materials:

(S)-2-[(S)-2-(1,4-dioxo-1,4-dihydronaphthalen-2-ylamino)-3-phenylpropanamido]-3-methylbutanoic acid

(S)-2-[(S)-2-(1,4-dioxo-1,4-dihydronaphthalen-2-ylamino)-3-phenylpropanamido]-3-(1H-indol-3-yl)propanoic acid

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