7,7-dimethylbicyclo[2.2.1]heptan-2-ol

Base Information

Chemical Name:7,7-dimethylbicyclo[2.2.1]heptan-2-ol
CAS No.:3588-22-5
Molecular Formula:C₉H₁₆O
Molecular Weight:140.225
Hs Code.:
Mol file:3588-22-5.mol

Synonyms:2-Norbornanol,7,7-dimethyl-, endo- (8CI); 7,7-Dimethyl-endo-norbornanol; NSC 147729; endo-a-Fenchocamphorol

Suppliers and Price of 7,7-dimethylbicyclo[2.2.1]heptan-2-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 7,7-dimethylbicyclo[2.2.1]heptan-2-ol

Chemical Property:

Vapor Pressure:0.069mmHg at 25°C
Boiling Point:203°C at 760 mmHg
Flash Point:78.8°C
Density:0.997g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 7,7-dimethylbicyclo[2.2.1]heptan-2-ol

There total 1 articles about 7,7-dimethylbicyclo[2.2.1]heptan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 514-15-8,32989-00-7,40550-41-2,110012-74-3
7,7-dimethylnorbornanone

: 611-70-1
phenyl isopropyl ketone

: 611-69-8
rac-2-methyl-1-phenylpropan-1-ol

: 3588-22-5,26908-71-4,30884-63-0,32989-04-1,51153-09-4,51153-10-7,91605-15-1,111821-63-7,111821-64-8
(1S,4S)-7,7-Dimethyl-bicyclo[2.2.1]heptan-2-ol

Guidance literature:: With bis(2,6-di-tert-butyl-4-methylphenoxide)methylaluminum; diisobutylaluminium hydride; at -78 ℃; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/ja00216a050

Reference yield: 99.0%

: 3588-22-5,26908-71-4,30884-63-0,32989-04-1,51153-09-4,51153-10-7,91605-15-1,111821-63-7,111821-64-8
(-)-borneol

: 514-15-8,32989-00-7,40550-41-2,110012-74-3
7,7-dimethylbicyclo[2.2.1]heptan-2-one

Guidance literature:: With ruthenium trichloride; iodobenzene; potassium peroxymonosulfate; In water; acetonitrile; at 20 ℃; for 0.8h; Inert atmosphere;
DOI:10.1016/j.tet.2010.04.046

Reference yield: 93.0%

: 3588-22-5,26908-71-4,30884-63-0,32989-04-1,51153-09-4,51153-10-7,91605-15-1,111821-63-7,111821-64-8
(-)-borneol

: phenylacetic acid

: C₂₀H₂₈O₂

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1021/jacs.5b08551