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Cyclobutanemethanol, 2,2-dimethyl-3-(1-methylethylidene)-, (1S)- (9CI)

Base Information Edit
  • Chemical Name:Cyclobutanemethanol, 2,2-dimethyl-3-(1-methylethylidene)-, (1S)- (9CI)
  • CAS No.:754227-25-3
  • Molecular Formula:C10H18O
  • Molecular Weight:154.252
  • Hs Code.:
  • Mol file:754227-25-3.mol
Cyclobutanemethanol, 2,2-dimethyl-3-(1-methylethylidene)-, (1S)- (9CI)

Synonyms:(S)-(+)-Maconelliol

Suppliers and Price of Cyclobutanemethanol, 2,2-dimethyl-3-(1-methylethylidene)-, (1S)- (9CI)
Supply Marketing:Edit
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
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Total 2 raw suppliers
Chemical Property of Cyclobutanemethanol, 2,2-dimethyl-3-(1-methylethylidene)-, (1S)- (9CI) Edit
Chemical Property:
  • PSA:20.23000 
  • LogP:2.36120 
Purity/Quality:
Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:

SDS file from LookChem

Useful:
Technology Process of Cyclobutanemethanol, 2,2-dimethyl-3-(1-methylethylidene)-, (1S)- (9CI)

There total 8 articles about Cyclobutanemethanol, 2,2-dimethyl-3-(1-methylethylidene)-, (1S)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With lithium aluminium tetrahydride; In diethyl ether; at 20 ℃;
DOI:10.1021/jf048198k
Guidance literature:
(R)-(-)-2,2-dimethyl-3-(1-methylethylidene)cyclobutanecarboxylic acid; With lithium aluminium tetrahydride; In diethyl ether; at 20 ℃; Inert atmosphere; Cooling with ice;
With water; sodium hydroxide; for 0.5h; Cooling with ice;
Guidance literature:
Multi-step reaction with 4 steps
1.1: MeLi / tetrahydrofuran; diethyl ether / 0.25 h / -20 °C
1.2: tetrahydrofuran; diethyl ether / 1.5 h / -10 - 20 °C
2.1: POCl3; pyridine / 24 h / 20 °C
3.1: p-toluenesulfonic acid / benzene / 24 h / Heating
4.1: 88 percent / LiAlH4 / diethyl ether / 20 °C
With pyridine; lithium aluminium tetrahydride; methyllithium; toluene-4-sulfonic acid; trichlorophosphate; In tetrahydrofuran; diethyl ether; benzene;
DOI:10.1021/jf048198k
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