Thioacetic acid S-((2R,3R,4S)-5-allyl-3,4-bis-benzyloxy-tetrahydro-furan-2-ylmethyl) ester

Base Information

Chemical Name:Thioacetic acid S-((2R,3R,4S)-5-allyl-3,4-bis-benzyloxy-tetrahydro-furan-2-ylmethyl) ester
CAS No.:592532-89-3
Molecular Formula:C₂₄H₂₈O₄S
Molecular Weight:412.55
Hs Code.:

Synonyms:Thioacetic acid S-((2R,3R,4S)-5-allyl-3,4-bis-benzyloxy-tetrahydro-furan-2-ylmethyl) ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Thioacetic acid S-((2R,3R,4S)-5-allyl-3,4-bis-benzyloxy-tetrahydro-furan-2-ylmethyl) ester

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Technology Process of Thioacetic acid S-((2R,3R,4S)-5-allyl-3,4-bis-benzyloxy-tetrahydro-furan-2-ylmethyl) ester

There total 4 articles about Thioacetic acid S-((2R,3R,4S)-5-allyl-3,4-bis-benzyloxy-tetrahydro-furan-2-ylmethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 592532-88-2
Methanesulfonic acid (2S,3S,4S)-5-allyl-3,4-bis-benzyloxy-tetrahydro-furan-2-ylmethyl ester

: 10387-40-3
potassium thioacetate

: 592532-89-3
Thioacetic acid S-((2R,3R,4S)-5-allyl-3,4-bis-benzyloxy-tetrahydro-furan-2-ylmethyl) ester

Guidance literature:: In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/S0040-4039(03)01039-6

Reference yield:

: 592532-87-1
3-(5-O-acetyl-2,3-di-O-benzyl-L-arabinofuranosyl)propene

: 592532-89-3
Thioacetic acid S-((2R,3R,4S)-5-allyl-3,4-bis-benzyloxy-tetrahydro-furan-2-ylmethyl) ester

Guidance literature:: Multi-step reaction with 3 steps

1: NaOMe / 2 h / 20 °C

2: 77 percent / pyridine / 0 - 22 °C

3: 62 percent / dimethylformamide / 20 °C

With sodium methylate; In pyridine; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(03)01039-6

Reference yield:

: allyl C-L-arabinoforanoside

: 592532-89-3
Thioacetic acid S-((2R,3R,4S)-5-allyl-3,4-bis-benzyloxy-tetrahydro-furan-2-ylmethyl) ester

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / aq. H₂SO₄ / 20 °C

2: NaOMe / 2 h / 20 °C

3: 77 percent / pyridine / 0 - 22 °C

4: 62 percent / dimethylformamide / 20 °C

With sulfuric acid; sodium methylate; In pyridine; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(03)01039-6