Technology Process of C52H72O6
There total 9 articles about C52H72O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
air; N,N,N,N,-tetramethylethylenediamine; copper(l) chloride;
In
xylene;
at 140 ℃;
DOI:10.1021/ol990567o
- Guidance literature:
-
Multi-step reaction with 2 steps
1: NaH / tetrahydrofuran / Heating
2: CuCl; TMEDA; air / xylene / 140 °C
With
air; N,N,N,N,-tetramethylethylenediamine; sodium hydride; copper(l) chloride;
In
tetrahydrofuran; xylene;
2: Glaser oxidation;
DOI:10.1021/ol990567o
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: Li; t-BuOK; 1,3-diaminopropane / 70 °C
1.2: Et3N / CH2Cl2
2.1: NaH / tetrahydrofuran / Heating
3.1: CuCl; TMEDA; air / xylene / 140 °C
With
air; N,N,N,N,-tetramethylethylenediamine; potassium tert-butylate; lithium; sodium hydride; Trimethylenediamine; copper(l) chloride;
In
tetrahydrofuran; xylene;
3.1: Glaser oxidation;
DOI:10.1021/ol990567o