Technology Process of C30H34O3
There total 6 articles about C30H34O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 5 h / 0 - 20 °C
2.1: Dess-Martin periodane / dichloromethane / 5 h / 0 °C
3.1: toluene / -78 °C / Molecular sieve
3.2: 0.5 h / 0 °C
4.1: pyridine; dmap / dichloromethane
With
pyridine; dmap; tetrabutyl ammonium fluoride; Dess-Martin periodane;
In
tetrahydrofuran; dichloromethane; toluene;
2.1: Dess-Martin oxidation / 3.1: Roush coupling / 3.2: Roush coupling;
DOI:10.1021/ol300182r
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: toluene / -78 °C / Molecular sieve
1.2: 0.5 h / 0 °C
2.1: pyridine; dmap / dichloromethane
With
pyridine; dmap;
In
dichloromethane; toluene;
1.1: Roush coupling / 1.2: Roush coupling;
DOI:10.1021/ol300182r
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: Dess-Martin periodane / dichloromethane / 5 h / 0 °C
2.1: toluene / -78 °C / Molecular sieve
2.2: 0.5 h / 0 °C
3.1: pyridine; dmap / dichloromethane
With
pyridine; dmap; Dess-Martin periodane;
In
dichloromethane; toluene;
1.1: Dess-Martin oxidation / 2.1: Roush coupling / 2.2: Roush coupling;
DOI:10.1021/ol300182r