N-tert-butyloxycarbonyl-O-benzyl glutamic nitrile

Base Information

Chemical Name:N-tert-butyloxycarbonyl-O-benzyl glutamic nitrile
CAS No.:1120367-12-5
Molecular Formula:C₁₇H₂₂N₂O₄
Molecular Weight:318.373
Hs Code.:

Synonyms:N-tert-butyloxycarbonyl-O-benzyl glutamic nitrile

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Chemical Property of N-tert-butyloxycarbonyl-O-benzyl glutamic nitrile

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Technology Process of N-tert-butyloxycarbonyl-O-benzyl glutamic nitrile

There total 2 articles about N-tert-butyloxycarbonyl-O-benzyl glutamic nitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 18800-73-2
benzyl N-tert-butyloxycarbonyl-L-γ-glutamate α-amide

: 1120367-12-5
N-tert-butyloxycarbonyl-O-benzyl glutamic nitrile

Guidance literature:: With 1,3,5-trichloro-2,4,6-triazine; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 22.5h;
DOI:10.1055/s-0028-1088128

Reference yield: 80.0%

: 1676-73-9,25014-27-1
L-glutamic acid γ-benzyl ester

: 24424-99-5
di-tert-butyl dicarbonate

: 1120367-12-5
N-tert-butyloxycarbonyl-O-benzyl glutamic nitrile

Guidance literature:: L-glutamic acid γ-benzyl ester; di-tert-butyl dicarbonate; With triethylamine; In 1,4-dioxane; water; at 20 ℃; Inert atmosphere;

With ammonia; chloroformic acid ethyl ester; triethylamine; In tetrahydrofuran; at 0 ℃; Inert atmosphere;

With triethylamine; trifluoroacetic anhydride; In tetrahydrofuran; at 0 ℃; Inert atmosphere;
DOI:10.1002/ejoc.201701477

Reference yield: 88.0%

: 1120367-12-5
N-tert-butyloxycarbonyl-O-benzyl glutamic nitrile

: 1120367-21-6
γ-benzyl N-tert-butyloxycarbonyl-L-glutamate α-tetrazole

Guidance literature:: With sodium azide; acetic acid; triethylamine; In toluene; for 16h; Inert atmosphere; Reflux;
DOI:10.1055/s-0028-1088128