O-(3-formylphenyl)dimethylthiocarbamate

Base Information

• Chemical Name: O-(3-formylphenyl)dimethylthiocarbamate
• CAS No.: 153561-34-3
• Molecular Formula: C₁₀H₁₁NO₂S
• Molecular Weight: 209.269
• Mol file: 153561-34-3.mol

Synonyms:O-(3-formylphenyl)dimethylthiocarbamate

Chemical Property of O-(3-formylphenyl)dimethylthiocarbamate

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of O-(3-formylphenyl)dimethylthiocarbamate

There total 1 articles about O-(3-formylphenyl)dimethylthiocarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

meta-hydroxybenzaldehyde (100-83-4) + N,N-Dimethylthiocarbamoyl chloride (16420-13-6) → O-(3-formylphenyl)dimethylthiocarbamate (153561-34-3)

Guidance literature:

With potassium hydroxide; In tetrahydrofuran; water; at 0 - 8 ℃; for 2h;

DOI:10.1039/c9cc09498a

Reference yield: 39.0%

O-(3-formylphenyl)dimethylthiocarbamate (153561-34-3) → C10H11NO2S

Guidance literature:

In 1-methyl-pyrrolidin-2-one; at 225 ℃; for 5h;

DOI:10.1039/c9cc09498a

Reference yield:

O-(3-formylphenyl)dimethylthiocarbamate (153561-34-3) → C12H17NO3S

Guidance literature:

Multi-step reaction with 2 steps

1: 1-methyl-pyrrolidin-2-one / 5 h / 225 °C

2: toluene-4-sulfonic acid / 1 h

With toluene-4-sulfonic acid; In 1-methyl-pyrrolidin-2-one;

DOI:10.1039/c9cc09498a

upstream raw materials:

meta-hydroxybenzaldehyde

N,N-Dimethylthiocarbamoyl chloride