N-[2-tert-butoxy-5-(trifluoromethyl)benzyl]-3-hydroxy-1-(1-hydroxyethyl)cyclopentanecarboxamide

Base Information

• Chemical Name: N-[2-tert-butoxy-5-(trifluoromethyl)benzyl]-3-hydroxy-1-(1-hydroxyethyl)cyclopentanecarboxamide
• CAS No.: 1056166-24-5
• Molecular Formula: C₂₀H₂₈F₃NO₄
• Molecular Weight: 403.442

Synonyms:N-[2-tert-butoxy-5-(trifluoromethyl)benzyl]-3-hydroxy-1-(1-hydroxyethyl)cyclopentanecarboxamide

Chemical Property of N-[2-tert-butoxy-5-(trifluoromethyl)benzyl]-3-hydroxy-1-(1-hydroxyethyl)cyclopentanecarboxamide

Chemical Property:

Purity/Quality:

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Technology Process of N-[2-tert-butoxy-5-(trifluoromethyl)benzyl]-3-hydroxy-1-(1-hydroxyethyl)cyclopentanecarboxamide

There total 1 articles about N-[2-tert-butoxy-5-(trifluoromethyl)benzyl]-3-hydroxy-1-(1-hydroxyethyl)cyclopentanecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-[2-tert-butoxy-5-(trifluoromethyl)benzyl]-1-(1-hydroxyethyl)-3-oxocyclopentanecarboxamide (782493-34-9) → N-[2-tert-butoxy-5-(trifluoromethyl)benzyl]-3-hydroxy-1-(1-hydroxyethyl)cyclopentanecarboxamide (1056166-24-5)

Guidance literature:

With sodium tetramethylborate; In methanol; for 0.333333h;

Reference yield:

N-[2-tert-butoxy-5-(trifluoromethyl)benzyl]-3-hydroxy-1-(1-hydroxyethyl)cyclopentanecarboxamide (1056166-24-5) + acetic anhydride (108-24-7) → 1-[3-(acetyloxy)-1-({[2-tert-butoxy-5-(trifluoromethyl)benzyl]amino}carbonyl)cyclopentyl]ethyl acetate (782493-35-0)

Guidance literature:

With dmap; triethylamine; In 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran; at 20 ℃; for 2.5h;

Reference yield:

N-[2-tert-butoxy-5-(trifluoromethyl)benzyl]-3-hydroxy-1-(1-hydroxyethyl)cyclopentanecarboxamide (1056166-24-5) + acetic anhydride (108-24-7) → 1-[3-(acetyloxy)-1-({[2-tert-butoxy-5-(trifluoromethyl)benzyl]amino}carbonyl)cyclopentyl]ethyl acetate + 1-[3-(acetyloxy)-1-({[2-tert-butoxy-5-(trifluoromethyl)benzyl]amino}carbonyl)cyclopentyl]ethyl acetate + 1-[3-(acetyloxy)-1-({[2-tert-butoxy-5-(trifluoromethyl)benzyl]amino}carbonyl)cyclopentyl]ethyl acetate + 1-[3-(acetyloxy)-1-({[2-tert-butoxy-5-(trifluoromethyl)benzyl]amino}carbonyl)cyclopentyl]ethyl acetate + 1-[3-(acetyloxy)-1-({[2-tert-butoxy-5-(trifluoromethyl)benzyl]amino}carbonyl)cyclopentyl]ethyl acetate + 1-[3-(acetyloxy)-1-({[2-tert-butoxy-5-(trifluoromethyl)benzyl]amino}carbonyl)cyclopentyl]ethyl acetate + 1-[3-(acetyloxy)-1-({[2-tert-butoxy-5-(trifluoromethyl)benzyl]amino}carbonyl)cyclopentyl]ethyl acetate + 1-[3-(acetyloxy)-1-({[2-tert-butoxy-5-(trifluoromethyl)benzyl]amino}carbonyl)cyclopentyl]ethyl acetate

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; for 2.5h;

upstream raw materials:

N-[2-tert-butoxy-5-(trifluoromethyl)benzyl]-1-(1-hydroxyethyl)-3-oxocyclopentanecarboxamide

Downstream raw materials:

1-[3-(acetyloxy)-1-({[2-tert-butoxy-5-(trifluoromethyl)benzyl]amino}carbonyl)cyclopentyl]ethyl acetate

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