(3aR)-6c-allyloxy-5c-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2-phenyl-(3ar,6ac)-3a,5,6,6a-tetrahydro-furo[3,2-d]oxazole

Base Information

• Chemical Name: (3aR)-6c-allyloxy-5c-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2-phenyl-(3ar,6ac)-3a,5,6,6a-tetrahydro-furo[3,2-d]oxazole
• CAS No.: 20770-75-6
• Molecular Formula: C₁₉H₂₃NO₅
• Molecular Weight: 345.395

Synonyms:(3aR)-6c-allyloxy-5c-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2-phenyl-(3ar,6ac)-3a,5,6,6a-tetrahydro-furo[3,2-d]oxazole

Chemical Property of (3aR)-6c-allyloxy-5c-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2-phenyl-(3ar,6ac)-3a,5,6,6a-tetrahydro-furo[3,2-d]oxazole

Chemical Property:

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Technology Process of (3aR)-6c-allyloxy-5c-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2-phenyl-(3ar,6ac)-3a,5,6,6a-tetrahydro-furo[3,2-d]oxazole

There total 3 articles about (3aR)-6c-allyloxy-5c-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2-phenyl-(3ar,6ac)-3a,5,6,6a-tetrahydro-furo[3,2-d]oxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5'.6'-O-Isopropyliden-2-phenyl-α-D-glucofuranol<2'.1':4.5>-Δ2-oxazolin (19949-65-6,23661-45-2,97673-37-5) + allyl bromide (106-95-6) → (3aR)-6c-allyloxy-5c-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2-phenyl-(3ar,6ac)-3a,5,6,6a-tetrahydro-furo[3,2-d]oxazole (20770-75-6)

Guidance literature:

With sodium hydroxide; In benzene;

DOI:10.1039/j39680001903

Reference yield:

→ (3aR)-6c-allyloxy-5c-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2-phenyl-(3ar,6ac)-3a,5,6,6a-tetrahydro-furo[3,2-d]oxazole (20770-75-6)

Guidance literature:

Hydroxid 1, NaH, Allylbromid;

DOI:10.1016/S0008-6215(00)80376-6

Reference yield:

→ (3aR)-6c-allyloxy-5c-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2-phenyl-(3ar,6ac)-3a,5,6,6a-tetrahydro-furo[3,2-d]oxazole (20770-75-6)

Guidance literature:

Hydroxid 1, 1.) NaH, 2.) Allylbromid;

DOI:10.1016/S0008-6215(00)80376-6

upstream raw materials:

5'.6'-O-Isopropyliden-2-phenyl-α-D-glucofuranol<2'.1':4.5>-Δ²-oxazolin

allyl bromide

Downstream raw materials:

benzyl 3-O-allyl-2-benzamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

N-{(4aR,6R,7R,8R,8aS)-6-Benzyloxy-2-phenyl-8-[((E)-propenyl)oxy]-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl}-benzamide

N-((2R,3R,4R,5S,6R)-4-Allyloxy-2-benzyloxy-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-3-yl)-benzamide

(1S,2R)-1-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2-(2-phenyl-oxazol-4-yl)-2-cis-propenyloxy-ethanol

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