methyl O-morpholinomethylphenylglyoxylate methyl maqnesiumchloride acetal

Base Information

• Chemical Name: methyl O-morpholinomethylphenylglyoxylate methyl maqnesiumchloride acetal
• CAS No.: 1072314-71-6
• Molecular Formula: C₁₅H₂₀NO₅*Cl*Mg
• Molecular Weight: 354.086

Synonyms:methyl O-morpholinomethylphenylglyoxylate methyl maqnesiumchloride acetal

Chemical Property of methyl O-morpholinomethylphenylglyoxylate methyl maqnesiumchloride acetal

Chemical Property:

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Technology Process of methyl O-morpholinomethylphenylglyoxylate methyl maqnesiumchloride acetal

There total 1 articles about methyl O-morpholinomethylphenylglyoxylate methyl maqnesiumchloride acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Dimethyl oxalate (553-90-2) + C11H14ClMgNO → methyl O-morpholinomethylphenylglyoxylate methyl maqnesiumchloride acetal (1072314-71-6)

Guidance literature:

In toluene; at -5 - 20 ℃; for 15h;

Reference yield: 30.3%

methyl O-morpholinomethylphenylglyoxylate methyl maqnesiumchloride acetal (1072314-71-6) → methyl [2-(chloromethyl)benzoyl]formate (130490-95-8)

Guidance literature:

With methyl chloroformate; In toluene; at 100 ℃; for 2h; under 9000.9 Torr;

Reference yield:

methyl O-morpholinomethylphenylglyoxylate methyl maqnesiumchloride acetal (1072314-71-6) → methyl O-morpholinemethylphenyl-gluoxylate (1072314-64-7)

Guidance literature:

With water; Purification / work up;

upstream raw materials:

Dimethyl oxalate

Downstream raw materials:

methyl [2-(chloromethyl)benzoyl]formate

methyl O-morpholinemethylphenyl-gluoxylate

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