C₁₉H₁₅NO

Base Information

• Chemical Name: C₁₉H₁₅NO
• CAS No.: 1451011-95-2
• Molecular Formula: C₁₉H₁₅NO
• Molecular Weight: 273.334
• Mol file: 1451011-95-2.mol

Synonyms:C₁₉H₁₅NO

Chemical Property of C₁₉H₁₅NO

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₁₉H₁₅NO

There total 3 articles about C₁₉H₁₅NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-1-Naphthalen-2-yl-3-(2-nitro-phenyl)-propenone (57221-66-6) → C19H15NO (1451011-95-2)

Guidance literature:

With hydrogenchloride; iron; In ethanol; water; Reflux;

DOI:10.1039/c6cc09430a

Reference yield:

2-nitro-benzaldehyde (552-89-6) → C19H15NO (1451011-95-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium hydroxide / ethanol / 20 °C

1.2: Reflux

2.1: iron; hydrogenchloride / ethanol; water / Reflux

With hydrogenchloride; iron; sodium hydroxide; In ethanol; water;

DOI:10.1039/c6cc09430a

Reference yield:

1-(naphthalen-2-yl)-2-(triphenylphosphoranylidene)ethanone (1777-59-9) → C19H15NO (1451011-95-2)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene / 90 °C

2: iron; acetic acid; hydrogenchloride / ethanol / 1 h / 25 °C

With hydrogenchloride; iron; acetic acid; In ethanol; toluene;

DOI:10.1039/c7ob01013c

upstream raw materials:

(E)-1-Naphthalen-2-yl-3-(2-nitro-phenyl)-propenone

2-nitro-benzaldehyde

1-(naphthalen-2-yl)-2-(triphenylphosphoranylidene)ethanone

Refernces

• 1、 Hu, Zhongyan,Dong, Jinhuan,Men, Yang,Li, Yifei,Xu, Xianxiu. "Organocatalyzed aerobic oxidative Robinson-type annulation of 2-isocyanochalcones: expedient synthesis of phenanthridines". supporting information. p. 1739 - 1742. Retrieved 2017/02/10.