PHOSPHORIC ACID 2-DIMETHYLAMINO-ETHYL ESTER 2,2-DIMETHYL-[1,3]DIOXOLAN-4-YLMETHYL ESTER METHYL ESTER

Base Information

Chemical Name:PHOSPHORIC ACID 2-DIMETHYLAMINO-ETHYL ESTER 2,2-DIMETHYL-[1,3]DIOXOLAN-4-YLMETHYL ESTER METHYL ESTER
CAS No.:77075-57-1
Molecular Formula:C₁₁H₂₄NO₆P
Molecular Weight:297.288
Hs Code.:2932999099
Mol file:77075-57-1.mol

Synonyms:PHOSPHORIC ACID 2-DIMETHYLAMINO-ETHYL ESTER 2,2-DIMETHYL-[1,3]DIOXOLAN-4-YLMETHYL ESTER METHYL ESTER

Suppliers and Price of PHOSPHORIC ACID 2-DIMETHYLAMINO-ETHYL ESTER 2,2-DIMETHYL-[1,3]DIOXOLAN-4-YLMETHYL ESTER METHYL ESTER

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
PHOSPHORIC ACID 2-DIMETHYLAMINO-ETHYL ESTER 2,2-DIMETHYL-(1,3)DIOXOLAN-4-YLMETHYL ESTER METHYL ESTER 95.00%
5MG
$ 504.39

Total 3 raw suppliers

Chemical Property of PHOSPHORIC ACID 2-DIMETHYLAMINO-ETHYL ESTER 2,2-DIMETHYL-[1,3]DIOXOLAN-4-YLMETHYL ESTER METHYL ESTER

Chemical Property:

Vapor Pressure:6.79E-05mmHg at 25°C
Refractive Index:1.444
Boiling Point:344°C at 760 mmHg
Flash Point:161.8°C
PSA：76.27000
Density:1.129g/cm³
LogP:1.48720

Purity/Quality:

99% ^*data from raw suppliers

PHOSPHORIC ACID 2-DIMETHYLAMINO-ETHYL ESTER 2,2-DIMETHYL-(1,3)DIOXOLAN-4-YLMETHYL ESTER METHYL ESTER 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of PHOSPHORIC ACID 2-DIMETHYLAMINO-ETHYL ESTER 2,2-DIMETHYL-[1,3]DIOXOLAN-4-YLMETHYL ESTER METHYL ESTER

There total 4 articles about PHOSPHORIC ACID 2-DIMETHYLAMINO-ETHYL ESTER 2,2-DIMETHYL-[1,3]DIOXOLAN-4-YLMETHYL ESTER METHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-79-8,36543-79-0
(R,S)-2,2-dimethyl-1,3-dioxolane-4-methanol

: 77075-57-1
methyl 2-(dimethylamino)ethyl 2,2-dimethyl-1,3-dioxolane-4-methyl phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: 2,6-lutidine / benzene / 1.) ice bath, 1,5 h, 2.) room temp., overnight

2: sodium / benzene

With 2,6-dimethylpyridine; sodium; In benzene;
DOI:10.1021/jo00174a012

Reference yield:

: 37616-36-7
sodium N,N-dimethylethanolamine

: methyl 2,2-dimethyl-1,3-dioxolane-4-methyl chlorophosphate

: 77075-57-1
methyl 2-(dimethylamino)ethyl 2,2-dimethyl-1,3-dioxolane-4-methyl phosphate

Guidance literature:: With sodium; In benzene; Yield given;
DOI:10.1021/jo00174a012

Reference yield:

: 100-79-8,36543-79-0
(R,S)-2,2-dimethyl-1,3-dioxolane-4-methanol

: 77075-57-1
methyl 2-(dimethylamino)ethyl 2,2-dimethyl-1,3-dioxolane-4-methyl phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: 2,6-lutidine / pentane / 0.5 h ice bath, room temp. overnight

2: diethyl ether; benzene / 1 h / ice bath

With 2,6-dimethylpyridine; In diethyl ether; pentane; benzene;
DOI:10.1016/S0040-4039(00)71474-2