C₃₄H₅₉N₃O₅Si

Base Information

Chemical Name:C₃₄H₅₉N₃O₅Si
CAS No.:922523-58-8
Molecular Formula:C₃₄H₅₉N₃O₅Si
Molecular Weight:617.945
Hs Code.:

C<sub>34</sub>H<sub>59</sub>N<sub>3</sub>O<sub>5</sub>Si

Synonyms:C₃₄H₅₉N₃O₅Si

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Chemical Property of C₃₄H₅₉N₃O₅Si

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Technology Process of C₃₄H₅₉N₃O₅Si

There total 17 articles about C₃₄H₅₉N₃O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 922523-38-4
C₃₇H₆₇N₃O₅Si₂

: 922523-58-8
C₃₄H₅₉N₃O₅Si

Guidance literature:: With tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; for 1h;
DOI:10.1002/anie.200603353

Reference yield:

: 922523-52-2
C₂₅H₃₅NO₄S

: 922523-58-8
C₃₄H₅₉N₃O₅Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: 89 percent / DIBAL-H / CH₂Cl₂ / 2 h

2.1: Et₃N; (cyclohexyl)2BOTf / CH₂Cl₂; hexane / 2.33 h

2.2: 86 percent / CH₂Cl₂ / 14 h / cooling

3.1: 17.1 mmol / NaH / various solvent(s) / 0.42 h

4.1: 75 percent / 2,6-lutidine / CH₂Cl₂ / 0.58 h

5.1: 98 percent / ceric ammonium nitrate / acetonitrile; H₂O / 1 h

6.1: 86 percent / 2,6-lutidine / CH₂Cl₂ / 0.5 h

7.1: 59 percent / diisobutylaluminium hydride / CH₂Cl₂ / -78 - 20 °C

8.1: 80 percent / Dess-Martin periodinane; NaHCO₃ / CH₂Cl₂ / 1 h / 20 °C

9.1: 94 percent / LDA / hexane; tetrahydrofuran / 0.25 h / cooling

10.1: 99 percent / tetra-n-butylammonium fluoride; acetic acid / tetrahydrofuran / 1 h

With 2,6-dimethylpyridine; ammonium cerium(IV) nitrate; tetrabutyl ammonium fluoride; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; acetic acid; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; hexane; dichloromethane; water; acetonitrile;
DOI:10.1002/anie.200603353

Reference yield:

: 922523-31-7
C₃₄H₄₂O₈

: 922523-58-8
C₃₄H₅₉N₃O₅Si

Guidance literature:: Multi-step reaction with 7 steps

1: 75 percent / 2,6-lutidine / CH₂Cl₂ / 0.58 h

2: 98 percent / ceric ammonium nitrate / acetonitrile; H₂O / 1 h

3: 86 percent / 2,6-lutidine / CH₂Cl₂ / 0.5 h

4: 59 percent / diisobutylaluminium hydride / CH₂Cl₂ / -78 - 20 °C

5: 80 percent / Dess-Martin periodinane; NaHCO₃ / CH₂Cl₂ / 1 h / 20 °C

6: 94 percent / LDA / hexane; tetrahydrofuran / 0.25 h / cooling

7: 99 percent / tetra-n-butylammonium fluoride; acetic acid / tetrahydrofuran / 1 h

With 2,6-dimethylpyridine; ammonium cerium(IV) nitrate; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; acetic acid; lithium diisopropyl amide; In tetrahydrofuran; hexane; dichloromethane; water; acetonitrile;
DOI:10.1002/anie.200603353