1,4-diacetyl-5-methyl-3-methylsulfonyl-5-phenyl-4,5-dihydro-1H-1,2,4-triazole

Base Information

Chemical Name:1,4-diacetyl-5-methyl-3-methylsulfonyl-5-phenyl-4,5-dihydro-1H-1,2,4-triazole
CAS No.:118807-26-4
Molecular Formula:C₁₄H₁₇N₃O₄S
Molecular Weight:323.373
Hs Code.:

Synonyms:1,4-diacetyl-5-methyl-3-methylsulfonyl-5-phenyl-4,5-dihydro-1H-1,2,4-triazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,4-diacetyl-5-methyl-3-methylsulfonyl-5-phenyl-4,5-dihydro-1H-1,2,4-triazole

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Technology Process of 1,4-diacetyl-5-methyl-3-methylsulfonyl-5-phenyl-4,5-dihydro-1H-1,2,4-triazole

There total 3 articles about 1,4-diacetyl-5-methyl-3-methylsulfonyl-5-phenyl-4,5-dihydro-1H-1,2,4-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 118807-47-9
1,4-diacetyl-5-methyl-3-methylthio-5-phenyl-4,5-dihydro-1H-1,2,4-triazole

: 118807-26-4
1,4-diacetyl-5-methyl-3-methylsulfonyl-5-phenyl-4,5-dihydro-1H-1,2,4-triazole

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In chloroform; for 24h; Ambient temperature; 2 eq. reagent;

Reference yield:

: 7575-81-7,56639-05-5,56639-27-1
acetophenone S-methylisothiosemicarbazone

: 118807-26-4
1,4-diacetyl-5-methyl-3-methylsulfonyl-5-phenyl-4,5-dihydro-1H-1,2,4-triazole

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / 2 h / Ambient temperature

2: 57 percent / 6 h / Heating

3: 94 percent / 80 percent m-CPBA / CHCl₃ / 24 h / Ambient temperature; 2 eq. reagent

With 3-chloro-benzenecarboperoxoic acid; In chloroform;

Reference yield:

: 118807-44-6
acetophenone 4-acetyl-3-methylisothiosemicarbazone

: 118807-26-4
1,4-diacetyl-5-methyl-3-methylsulfonyl-5-phenyl-4,5-dihydro-1H-1,2,4-triazole

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / 6 h / Heating

2: 94 percent / 80 percent m-CPBA / CHCl₃ / 24 h / Ambient temperature; 2 eq. reagent

With 3-chloro-benzenecarboperoxoic acid; In chloroform;