N₁-p-acetamidobenzyl-N₃-n-propyl-6-amino-5-p-carboxymethyloxybenzylideniminouracil

Base Information

• Chemical Name: N₁-p-acetamidobenzyl-N₃-n-propyl-6-amino-5-p-carboxymethyloxybenzylideniminouracil
• CAS No.: 220419-59-0
• Molecular Formula: C₂₅H₂₇N₅O₆
• Molecular Weight: 493.519

Synonyms:N₁-p-acetamidobenzyl-N₃-n-propyl-6-amino-5-p-carboxymethyloxybenzylideniminouracil

Chemical Property of N₁-p-acetamidobenzyl-N₃-n-propyl-6-amino-5-p-carboxymethyloxybenzylideniminouracil

Chemical Property:

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Technology Process of N₁-p-acetamidobenzyl-N₃-n-propyl-6-amino-5-p-carboxymethyloxybenzylideniminouracil

There total 7 articles about N₁-p-acetamidobenzyl-N₃-n-propyl-6-amino-5-p-carboxymethyloxybenzylideniminouracil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-p-nitrobenzyl-N'-n-propylurea → N1-p-acetamidobenzyl-N3-n-propyl-6-amino-5-p-carboxymethyloxybenzylideniminouracil (220419-59-0)

Guidance literature:

Multi-step reaction with 7 steps

1: 74 percent / Ac₂O / 20 h / 50 °C

2: 92 percent / conc NaOH / ethanol / 1 h

3: H₂ / PtO₂ / ethanol / 3 h / 760 Torr / Ambient temperature

4: 91 percent / pyridine / 2 h / 0 °C

5: 89 percent / NaNO₂ / methanol; acetic acid; H₂O / 3 h / Ambient temperature

6: H₂ / Raney Ni / ethanol / 4 h / 760 Torr / Ambient temperature

7: ethanol

With sodium hydroxide; hydrogen; acetic anhydride; sodium nitrite; platinum(IV) oxide; nickel; In pyridine; methanol; ethanol; water; acetic acid;

Reference yield:

N1-p-aminobenzyl-N3-n-propyl-6-aminouracil → N1-p-acetamidobenzyl-N3-n-propyl-6-amino-5-p-carboxymethyloxybenzylideniminouracil (220419-59-0)

Guidance literature:

Multi-step reaction with 4 steps

1: 91 percent / pyridine / 2 h / 0 °C

2: 89 percent / NaNO₂ / methanol; acetic acid; H₂O / 3 h / Ambient temperature

3: H₂ / Raney Ni / ethanol / 4 h / 760 Torr / Ambient temperature

4: ethanol

With hydrogen; sodium nitrite; nickel; In pyridine; methanol; ethanol; water; acetic acid;

Reference yield:

N-cyanoacetyl-N-n-propyl-N'-p-nitrobenzylurea → N1-p-acetamidobenzyl-N3-n-propyl-6-amino-5-p-carboxymethyloxybenzylideniminouracil (220419-59-0)

Guidance literature:

Multi-step reaction with 6 steps

1: 92 percent / conc NaOH / ethanol / 1 h

2: H₂ / PtO₂ / ethanol / 3 h / 760 Torr / Ambient temperature

3: 91 percent / pyridine / 2 h / 0 °C

4: 89 percent / NaNO₂ / methanol; acetic acid; H₂O / 3 h / Ambient temperature

5: H₂ / Raney Ni / ethanol / 4 h / 760 Torr / Ambient temperature

6: ethanol

With sodium hydroxide; hydrogen; sodium nitrite; platinum(IV) oxide; nickel; In pyridine; methanol; ethanol; water; acetic acid;

upstream raw materials:

(4-formylphenoxy)acetic acid

N₁-p-acetamidobenzyl-N₃-n-propyl-5,6-diaminouracil

Downstream raw materials:

N₃-p-acetamidobenzyl-N₁-n-propyl-8-p-carboxymethyloxyphenylxanthine

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