N,N'-Dibenzyl-N''-[(1R,6S)-6-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-4-methyl-1-vinyl-cyclohex-3-enyl]-guanidine

Base Information

Chemical Name:N,N'-Dibenzyl-N''-[(1R,6S)-6-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-4-methyl-1-vinyl-cyclohex-3-enyl]-guanidine
CAS No.:162089-67-0
Molecular Formula:C₂₉H₃₇N₃O₂
Molecular Weight:459.632
Hs Code.:

Synonyms:N,N'-Dibenzyl-N''-[(1R,6S)-6-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-4-methyl-1-vinyl-cyclohex-3-enyl]-guanidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-Dibenzyl-N''-[(1R,6S)-6-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-4-methyl-1-vinyl-cyclohex-3-enyl]-guanidine

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Technology Process of N,N'-Dibenzyl-N''-[(1R,6S)-6-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-4-methyl-1-vinyl-cyclohex-3-enyl]-guanidine

There total 6 articles about N,N'-Dibenzyl-N''-[(1R,6S)-6-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-4-methyl-1-vinyl-cyclohex-3-enyl]-guanidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: Benzyl-[(1R,6S)-6-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-4-methyl-1-vinyl-cyclohex-3-enyl]-carbodiimide

: 100-46-9
benzylamine

: 162089-67-0
N,N'-Dibenzyl-N''-[(1R,6S)-6-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-4-methyl-1-vinyl-cyclohex-3-enyl]-guanidine

Guidance literature:: With scandium tris(trifluoromethanesulfonate); In dichloromethane;
DOI:10.1246/cl.1994.2299

Reference yield:

: 162089-63-6
2-[(S)-6-((S)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-4-methyl-cyclohex-3-en-(Z)-ylidene]-ethanol

: 162089-67-0
N,N'-Dibenzyl-N''-[(1R,6S)-6-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-4-methyl-1-vinyl-cyclohex-3-enyl]-guanidine

Guidance literature:: Multi-step reaction with 5 steps

1: NaH / diethyl ether

2: xylene / Heating

3: 75 percent / Na₂CO₃ / dimethylformamide / 80 °C

4: 97 percent / PPh₃, CBr₄, Et₃N

5: 79 percent / Sc(OTf)3 / CH₂Cl₂

With carbon tetrabromide; sodium hydride; sodium carbonate; triethylamine; triphenylphosphine; scandium tris(trifluoromethanesulfonate); In diethyl ether; dichloromethane; N,N-dimethyl-formamide; xylene;
DOI:10.1246/cl.1994.2299

Reference yield:

: 199801-72-4
2,2,2-Trichloro-acetimidic acid 2-[(S)-6-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-4-methyl-cyclohex-3-en-(Z)-ylidene]-ethyl ester

: 162089-67-0
N,N'-Dibenzyl-N''-[(1R,6S)-6-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-4-methyl-1-vinyl-cyclohex-3-enyl]-guanidine

Guidance literature:: Multi-step reaction with 4 steps

1: xylene / Heating

2: 75 percent / Na₂CO₃ / dimethylformamide / 80 °C

3: 97 percent / PPh₃, CBr₄, Et₃N

4: 79 percent / Sc(OTf)3 / CH₂Cl₂

With carbon tetrabromide; sodium carbonate; triethylamine; triphenylphosphine; scandium tris(trifluoromethanesulfonate); In dichloromethane; N,N-dimethyl-formamide; xylene;
DOI:10.1246/cl.1994.2299