Technology Process of C50H60O12
There total 8 articles about C50H60O12 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
N,N-dimethyl-formamide;
at 80 ℃;
for 8h;
Inert atmosphere;
DOI:10.1021/ja806524m
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium hydroxide / tetrahydrofuran; water / 0 °C
2: potassium carbonate / N,N-dimethyl-formamide / 4 h / 70 °C / Inert atmosphere
3: lithium aluminium tetrahydride / tetrahydrofuran / 2.5 h / 0 - 20 °C / Inert atmosphere
4: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 0 - 20 °C / Inert atmosphere
5: potassium carbonate / N,N-dimethyl-formamide / 8 h / 80 °C / Inert atmosphere
With
sodium hydroxide; lithium aluminium tetrahydride; thionyl chloride; potassium carbonate; N,N-dimethyl-formamide;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja806524m
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 70 °C / Inert atmosphere
2: lithium aluminium tetrahydride / tetrahydrofuran / 2.5 h / 0 - 20 °C / Inert atmosphere
3: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 0 - 20 °C / Inert atmosphere
4: potassium carbonate / N,N-dimethyl-formamide / 8 h / 80 °C / Inert atmosphere
With
lithium aluminium tetrahydride; thionyl chloride; potassium carbonate; N,N-dimethyl-formamide;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja806524m
