PhMe₂SiC₆H₄C₆H₄B(pinacolato)

Base Information

• Chemical Name: PhMe₂SiC₆H₄C₆H₄B(pinacolato)
• CAS No.: 1316335-60-0
• Molecular Formula: C₂₆H₃₁BO₂Si
• Molecular Weight: 414.427
• Mol file: 1316335-60-0.mol

Synonyms:PhMe₂SiC₆H₄C₆H₄B(pinacolato)

Chemical Property of PhMe₂SiC₆H₄C₆H₄B(pinacolato)

Chemical Property:

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Technology Process of PhMe₂SiC₆H₄C₆H₄B(pinacolato)

There total 1 articles about PhMe₂SiC₆H₄C₆H₄B(pinacolato) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

bisbenzocyclobutene (259-79-0) + dimethylphenyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)silane (185990-03-8) → PhMe2SiC6H4C6H4B(pinacolato) (1316335-60-0)

Guidance literature:

With (CH₃)2NC₆H₄C₆H₄P(C(CH₃)3)2; Pd(C₆H₅CHCHCOCHCHC₆H₅)2; In toluene; reaction of biphenylene with 2 equiv. of borane deriv. in presence of palladium compd. and phosphine deriv. in toluene at 110°C for 5 h;

DOI:10.1021/om200436d

upstream raw materials:

bisbenzocyclobutene

dimethylphenyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)silane