C₂₉H₄₄O₄S₂

Base Information

Chemical Name:C₂₉H₄₄O₄S₂
CAS No.:1372122-80-9
Molecular Formula:C₂₉H₄₄O₄S₂
Molecular Weight:520.798
Hs Code.:

C<sub>29</sub>H<sub>44</sub>O<sub>4</sub>S<sub>2</sub>

Synonyms:C₂₉H₄₄O₄S₂

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Chemical Property of C₂₉H₄₄O₄S₂

Chemical Property:

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Technology Process of C₂₉H₄₄O₄S₂

There total 8 articles about C₂₉H₄₄O₄S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1372122-70-7
C₂₀H₂₆O₄

: 71547-56-3
2-(3-Methylbutyl)-1,3-dithiane

: 1372122-80-9
C₂₉H₄₄O₄S₂

Guidance literature:: 2-(3-Methylbutyl)-1,3-dithiane; With n-butyllithium; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at -78 ℃; for 0.666667h; Inert atmosphere;

C₂₀H₂₆O₄; With cerium(III) chloride bis(lithium chloride); In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at -78 ℃; Inert atmosphere;
DOI:10.1021/ol3007259

Reference yield:

: 1372122-72-9
C₂₃H₃₁NO₂S₂

: 1372122-80-9
C₂₉H₄₄O₄S₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: methanol; lithium borohydride / diethyl ether / 0 - 20 °C

2.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 2 h / 40 °C / Inert atmosphere

3.1: osmium(VIII) oxide; N,N,N,N,-tetramethylethylenediamine / dichloromethane / 14 h / -78 °C / Inert atmosphere

4.1: toluene-4-sulfonic acid / dichloromethane / 12 h / Inert atmosphere

5.1: tetrapropylammonium perruthenate; 4-methylmorpholine N-oxide / dichloromethane / 3 h / Inert atmosphere; Molecular sieve

6.1: n-butyllithium / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide / 0.67 h / -78 °C / Inert atmosphere

6.2: -78 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; methanol; osmium(VIII) oxide; lithium borohydride; n-butyllithium; tetrapropylammonium perruthenate; N,N,N,N,-tetramethylethylenediamine; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; dichloromethane;
DOI:10.1021/ol3007259

Reference yield:

: 1372122-75-2
C₁₅H₂₂O₄

: 1372122-80-9
C₂₉H₄₄O₄S₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: toluene-4-sulfonic acid / dichloromethane / 12 h / Inert atmosphere

2.1: tetrapropylammonium perruthenate; 4-methylmorpholine N-oxide / dichloromethane / 3 h / Inert atmosphere; Molecular sieve

3.1: n-butyllithium / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide / 0.67 h / -78 °C / Inert atmosphere

3.2: -78 °C / Inert atmosphere

With n-butyllithium; tetrapropylammonium perruthenate; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane;
DOI:10.1021/ol3007259