(Co(NH₃)5(NHSO₂C₆H₄NO₂))⁽²⁺⁾*2ClO₄^(1-)*H₂O=(Co(NH₃)5(NHSO₂C₆H₄NO₂))(ClO₄)2*H₂O

Base Information

• Chemical Name: (Co(NH₃)5(NHSO₂C₆H₄NO₂))⁽²⁺⁾*2ClO₄^(1-)*H₂O=(Co(NH₃)5(NHSO₂C₆H₄NO₂))(ClO₄)2*H₂O
• CAS No.: 78891-45-9
• Molecular Formula: C₆H₂₀CoN₇O₄S*2ClO₄*H₂O
• Molecular Weight: 562.245
• Mol file: 78891-45-9.mol

Synonyms:(Co(NH₃)5(NHSO₂C₆H₄NO₂))⁽²⁺⁾*2ClO₄^(1-)*H₂O=(Co(NH₃)5(NHSO₂C₆H₄NO₂))(ClO₄)2*H₂O

Chemical Property of (Co(NH₃)5(NHSO₂C₆H₄NO₂))⁽²⁺⁾*2ClO₄^(1-)*H₂O=(Co(NH₃)5(NHSO₂C₆H₄NO₂))(ClO₄)2*H₂O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (Co(NH₃)5(NHSO₂C₆H₄NO₂))⁽²⁺⁾*2ClO₄^(1-)*H₂O=(Co(NH₃)5(NHSO₂C₆H₄NO₂))(ClO₄)2*H₂O

There total 1 articles about (Co(NH₃)5(NHSO₂C₆H₄NO₂))⁽²⁺⁾*2ClO₄^(1-)*H₂O=(Co(NH₃)5(NHSO₂C₆H₄NO₂))(ClO₄)2*H₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

aquapentaamminecobalt(III) perchlorate (13820-81-0) + p-nitrobenzenesulfonamide (6325-93-5) + sodium perchlorate → (Co(NH3)5(NHSO2C6H4NO2))(2+)*2ClO4(1-)*H2O=(Co(NH3)5(NHSO2C6H4NO2))(ClO4)2*H2O (78891-45-9)

Guidance literature:

With 2,6-dimethylpyridine; In N,N-dimethyl acetamide; soln. (Co(NH3)5(H2O))(ClO4)3 in dry dimethylacetamide mixed with soln. p-nitrobenzenesulfonamide and 2,6-lutidine in dimethylacetamide, soln. heated for 3 h on steam bath, cooled, filtered, solvent ext. with ether, oil dissolved in water, NaClO4 added; product purified by ion-exchange chromy. on Baker CGC-271 in Na(1+) form (eluted with NaClO4 soln., product at the top column separated, washedwith water, acetic acid), NaOH and NaClO4 added, complex recrystd. fromwater, washed with ether; elem. anal.;

DOI:10.1021/ic00133a003

Reference yield:

(Co(NH3)5(NHSO2C6H4NO2))(2+)*2ClO4(1-)*H2O=(Co(NH3)5(NHSO2C6H4NO2))(ClO4)2*H2O (78891-45-9) → aquapentaamminecobalt(III) perchlorate (13820-81-0) + p-nitrobenzenesulfonamide (6325-93-5)

Guidance literature:

With water; In water; hydrolysis sulfamido complex in aq. acidic soln.; Kinetics;

DOI:10.1021/ic00133a003

upstream raw materials:

aquapentaamminecobalt(III) perchlorate

p-nitrobenzenesulfonamide

Downstream raw materials:

aquapentaamminecobalt(III) perchlorate

p-nitrobenzenesulfonamide

Refernces