3-[(N-benzyloxycarbonyl)amino]propyl-O-(4-azido-3-O-benzyl-4,6-dideoxy-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside

Base Information

Chemical Name:3-[(N-benzyloxycarbonyl)amino]propyl-O-(4-azido-3-O-benzyl-4,6-dideoxy-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside
CAS No.:927680-49-7
Molecular Formula:C₆₄H₇₀N₄O₁₆
Molecular Weight:1151.28
Hs Code.:

3-[(N-benzyloxycarbonyl)amino]propyl-O-(4-azido-3-O-benzyl-4,6-dideoxy-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside

Synonyms:3-[(N-benzyloxycarbonyl)amino]propyl-O-(4-azido-3-O-benzyl-4,6-dideoxy-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside

Suppliers and Price of 3-[(N-benzyloxycarbonyl)amino]propyl-O-(4-azido-3-O-benzyl-4,6-dideoxy-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-[(N-benzyloxycarbonyl)amino]propyl-O-(4-azido-3-O-benzyl-4,6-dideoxy-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-[(N-benzyloxycarbonyl)amino]propyl-O-(4-azido-3-O-benzyl-4,6-dideoxy-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside

There total 13 articles about 3-[(N-benzyloxycarbonyl)amino]propyl-O-(4-azido-3-O-benzyl-4,6-dideoxy-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 927680-48-6
3-[(N-benzyloxycarbonyl)amino]propyl-O-(4-azido-3-O-benzyl-4,6-dideoxy-2-O-levulinoyl-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside

: 927680-49-7
3-[(N-benzyloxycarbonyl)amino]propyl-O-(4-azido-3-O-benzyl-4,6-dideoxy-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: With hydrazinium monoacetate; In methanol; dichloromethane; at 20 ℃; for 4h;
DOI:10.1002/chem.200601245

Reference yield:

: 142776-67-8
ethyl 2-O-benzoyl-4-O-benzyl-1-thio-α-L-rhamnopyranoside

: 927680-49-7
3-[(N-benzyloxycarbonyl)amino]propyl-O-(4-azido-3-O-benzyl-4,6-dideoxy-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 72 percent / 4 Angstroem molecular sieves; N-iodosuccinimide; trifluoromethaneulfonic acid / CH₂Cl₂ / 0 °C

2: 78 percent / 4 Angstroem molecular sieves; N-iodosuccinimide; trifluoromethaneulfonic acid / CH₂Cl₂ / 0 °C

3: 93 percent / hyrazine acetate / methanol; CH₂Cl₂ / 4 h / 20 °C

4: 76 percent / 4 Angstroem molecular sieves; N-iodosuccinimide; trifluoromethaneulfonic acid / CH₂Cl₂ / 0 °C

5: 93 percent / hyrazine acetate / methanol; CH₂Cl₂ / 4 h / 20 °C

With N-iodo-succinimide; trifluorormethanesulfonic acid; 4 A molecular sieve; hydrazinium monoacetate; In methanol; dichloromethane;
DOI:10.1002/chem.200601245

Reference yield:

: 927680-41-9
ethyl 3,4-O-isopropylidene-2-O-levulinoyl-1-thio-β-D-fucopyranoside

: 927680-49-7
3-[(N-benzyloxycarbonyl)amino]propyl-O-(4-azido-3-O-benzyl-4,6-dideoxy-β-D-glucopyranosyl)-(1->3)-O-(2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1.1: 100 percent / aq. acetic acid / 0.25 h / 90 °C

2.1: dibutyltin oxide / toluene / 3 h / Heating

2.2: 52 percent / tetrabutylammonium bromide / toluene / 3 h / Heating

3.1: pyridine / CH₂Cl₂ / 1 h / 0 °C

4.1: 0.42 g / sodium azide / dimethylformamide / 40 °C

5.1: 76 percent / 4 Angstroem molecular sieves; N-iodosuccinimide; trifluoromethaneulfonic acid / CH₂Cl₂ / 0 °C

6.1: 93 percent / hyrazine acetate / methanol; CH₂Cl₂ / 4 h / 20 °C

With pyridine; N-iodo-succinimide; sodium azide; trifluorormethanesulfonic acid; 4 A molecular sieve; hydrazinium monoacetate; di(n-butyl)tin oxide; acetic acid; In methanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1002/chem.200601245