2,3-bis-O-(phenylmethyl)-4,6-O-[(R)-phenylmethylene]-α-D-mannopyranoside

Base Information

Chemical Name:2,3-bis-O-(phenylmethyl)-4,6-O-[(R)-phenylmethylene]-α-D-mannopyranoside
CAS No.:154172-24-4
Molecular Formula:C₂₇H₂₈O₆
Molecular Weight:448.516
Hs Code.:

Synonyms:2,3-bis-O-(phenylmethyl)-4,6-O-[(R)-phenylmethylene]-α-D-mannopyranoside

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Chemical Property of 2,3-bis-O-(phenylmethyl)-4,6-O-[(R)-phenylmethylene]-α-D-mannopyranoside

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Technology Process of 2,3-bis-O-(phenylmethyl)-4,6-O-[(R)-phenylmethylene]-α-D-mannopyranoside

There total 16 articles about 2,3-bis-O-(phenylmethyl)-4,6-O-[(R)-phenylmethylene]-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 119237-86-4
allyl 2,3-di-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside

: 154172-24-4
2,3-bis-O-(phenylmethyl)-4,6-O-[(R)-phenylmethylene]-α-D-mannopyranoside

Guidance literature:: With selenium(IV) oxide; In acetic acid;
DOI:10.1016/j.tetlet.2004.03.135

Reference yield:

: acetyl 2,3-di-O-benzyl-4,6-O-benzylidene-β-D-mannopyranoside

: 2,3-di-O-benzyl-4,6-O-benzylidene-β-D-mannopyranose

: 154172-24-4
2,3-bis-O-(phenylmethyl)-4,6-O-[(R)-phenylmethylene]-α-D-mannopyranoside

Guidance literature:: acetyl 2,3-di-O-benzyl-4,6-O-benzylidene-β-D-mannopyranoside; With potassium tert-butylate; In methanol; at -30 - 0 ℃; for 1h;

In chloroform-d1; for 24h; optical yield given as %de;
DOI:10.1016/j.carres.2012.05.025

Reference yield:

: acetyl 2,3-di-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside

: 2,3-di-O-benzyl-4,6-O-benzylidene-β-D-mannopyranose

: 154172-24-4
2,3-bis-O-(phenylmethyl)-4,6-O-[(R)-phenylmethylene]-α-D-mannopyranoside

Guidance literature:: acetyl 2,3-di-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside; With potassium tert-butylate; In methanol; at -30 - 0 ℃; for 1h;

In chloroform-d1; for 24h; optical yield given as %de;
DOI:10.1016/j.carres.2012.05.025