2'-O-acetyl-erythromycin A (9E)-O-(1-isopropoxycyclohex-1-yl)oxime-11,12-carbonate

Base Information

• Chemical Name: 2'-O-acetyl-erythromycin A (9E)-O-(1-isopropoxycyclohex-1-yl)oxime-11,12-carbonate
• CAS No.: 887125-84-0
• Molecular Formula: C₄₉H₈₄N₂O₁₆
• Molecular Weight: 957.21

Synonyms:2'-O-acetyl-erythromycin A (9E)-O-(1-isopropoxycyclohex-1-yl)oxime-11,12-carbonate

Chemical Property of 2'-O-acetyl-erythromycin A (9E)-O-(1-isopropoxycyclohex-1-yl)oxime-11,12-carbonate

Chemical Property:

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Technology Process of 2'-O-acetyl-erythromycin A (9E)-O-(1-isopropoxycyclohex-1-yl)oxime-11,12-carbonate

There total 1 articles about 2'-O-acetyl-erythromycin A (9E)-O-(1-isopropoxycyclohex-1-yl)oxime-11,12-carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2'-O-acetylerythromycin A (9E)-(1-isopropoxycychex-1-yl)oxime (887125-82-8) + bis(trichloromethyl) carbonate (32315-10-9) → 2'-O-acetyl-erythromycin A (9E)-O-(1-isopropoxycyclohex-1-yl)oxime-11,12-carbonate (887125-84-0)

Guidance literature:

With pyridine; In dichloromethane; at 0 ℃; for 1h;

Reference yield:

2'-O-acetyl-erythromycin A (9E)-O-(1-isopropoxycyclohex-1-yl)oxime-11,12-carbonate (887125-84-0) + tert-butyl allyl carbonate (70122-89-3) → 2'-O-acetyl-4''-O-allylerythromycin A (9E)-O-(1-isopropoxycyclohex-1-yl)oxime-11,12-carbonate (887125-86-2)

Guidance literature:

tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; for 2h; Heating / reflux;

upstream raw materials:

2'-O-acetylerythromycin A (9E)-(1-isopropoxycychex-1-yl)oxime

bis(trichloromethyl) carbonate

Downstream raw materials:

2'-O-acetyl-4''-O-allylerythromycin A (9E)-O-(1-isopropoxycyclohex-1-yl)oxime-11,12-carbonate

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