Technology Process of C34H34N2O3
There total 14 articles about C34H34N2O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium bis(2-methoxyethoxy)aluminium dihydride;
In
tetrahydrofuran;
Heating;
DOI:10.1021/ja991714g
- Guidance literature:
-
Multi-step reaction with 10 steps
1: 92 percent / Me3Al / toluene / 20 °C
2: 87 percent / NaH / dimethylformamide
3: 70 percent / BCl3 / -78 °C
4: 86 percent / imidazole / CH2Cl2
5: 71 percent / (Ph3P)2PdCl2; Et3N / N,N-dimethyl-acetamide / 100 °C
6: HF / acetonitrile
7: NaBH4 / methanol
8: Pb(OAc)4 / benzene
9: NaBH4 / methanol
10: sodium bis(2-methoxyethoxy)aluminum hydride / tetrahydrofuran / Heating
With
1H-imidazole; lead(IV) acetate; bis-triphenylphosphine-palladium(II) chloride; sodium tetrahydroborate; hydrogen fluoride; trimethylaluminum; boron trichloride; sodium hydride; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl acetamide; N,N-dimethyl-formamide; toluene; acetonitrile; benzene;
1: Condensation / 2: N-benzylation / 3: debenzylation / 4: silylation / 5: Cyclization / 6: desilylation / 7: Reduction / 8: Ring cleavage / 9: Reduction / 10: Reduction;
DOI:10.1021/ja991714g
- Guidance literature:
-
Multi-step reaction with 2 steps
1: NaBH4 / methanol
2: sodium bis(2-methoxyethoxy)aluminum hydride / tetrahydrofuran / Heating
With
sodium tetrahydroborate; sodium bis(2-methoxyethoxy)aluminium dihydride;
In
tetrahydrofuran; methanol;
1: Reduction / 2: Reduction;
DOI:10.1021/ja991714g