5-({4-[2-(hydroxyimino)-2-(3-methoxyphenyl)ethoxy]phenyl}methyl)-2,4-thiazolidinedione

Base Information

Chemical Name:5-({4-[2-(hydroxyimino)-2-(3-methoxyphenyl)ethoxy]phenyl}methyl)-2,4-thiazolidinedione
CAS No.:1359826-34-8
Molecular Formula:C₁₉H₁₈N₂O₅S
Molecular Weight:386.428
Hs Code.:

Synonyms:5-({4-[2-(hydroxyimino)-2-(3-methoxyphenyl)ethoxy]phenyl}methyl)-2,4-thiazolidinedione

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Chemical Property of 5-({4-[2-(hydroxyimino)-2-(3-methoxyphenyl)ethoxy]phenyl}methyl)-2,4-thiazolidinedione

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Technology Process of 5-({4-[2-(hydroxyimino)-2-(3-methoxyphenyl)ethoxy]phenyl}methyl)-2,4-thiazolidinedione

There total 5 articles about 5-({4-[2-(hydroxyimino)-2-(3-methoxyphenyl)ethoxy]phenyl}methyl)-2,4-thiazolidinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1359826-33-7
(5Z)-5-(4-(2-(hydroxyimino)-2-(3-methoxyphenyl)ethoxy)benzylidene)thiazolidine-2,4-dione

: 1359826-34-8
5-({4-[2-(hydroxyimino)-2-(3-methoxyphenyl)ethoxy]phenyl}methyl)-2,4-thiazolidinedione

Guidance literature:: (5Z)-5-(4-(2-(hydroxyimino)-2-(3-methoxyphenyl)ethoxy)benzylidene)thiazolidine-2,4-dione; With [2,2]bipyridinyl; cobalt(II) chloride hexahydrate; In tetrahydrofuran; water; at 20 ℃; for 0.166667h;

With sodium tetrahydroborate; water; In tetrahydrofuran; at 20 ℃;

With acetic acid; In tetrahydrofuran; water; pH=6 - 7;

Reference yield:

: 103788-60-9,154052-92-3
5-[(4-hydroxyphenyl)methylene]-2,4-thiazolidinedione

: 1359826-34-8
5-({4-[2-(hydroxyimino)-2-(3-methoxyphenyl)ethoxy]phenyl}methyl)-2,4-thiazolidinedione

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium tert-butylate / dimethyl sulfoxide / 1 h / 20 °C

1.2: 2 h

2.1: hydroxylamine hydrochloride / N,N-dimethyl-formamide; tetrahydrofuran / 20 °C

3.1: [2,2]bipyridinyl; cobalt(II) chloride hexahydrate / water; tetrahydrofuran / 0.17 h / 20 °C

3.2: 20 °C

3.3: pH 6 - 7

With [2,2]bipyridinyl; cobalt(II) chloride hexahydrate; hydroxylamine hydrochloride; potassium tert-butylate; In tetrahydrofuran; water; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 1359826-32-6
(Z)-5-(4-(2-(3-methoxyphenyl)-2-oxoethoxy)benzylidene)thiazolidine-2,4-dione

: 1359826-34-8
5-({4-[2-(hydroxyimino)-2-(3-methoxyphenyl)ethoxy]phenyl}methyl)-2,4-thiazolidinedione

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydroxylamine hydrochloride / N,N-dimethyl-formamide; tetrahydrofuran / 20 °C

2.1: [2,2]bipyridinyl; cobalt(II) chloride hexahydrate / water; tetrahydrofuran / 0.17 h / 20 °C

2.2: 20 °C

2.3: pH 6 - 7

With [2,2]bipyridinyl; cobalt(II) chloride hexahydrate; hydroxylamine hydrochloride; In tetrahydrofuran; water; N,N-dimethyl-formamide;