Technology Process of C56H70O6
There total 5 articles about C56H70O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 0 ℃;
for 0.0833333h;
Inert atmosphere;
Darkness;
DOI:10.1021/ma101816z
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.08 h / 0 °C / Inert atmosphere; Darkness
2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / ethyl acetate / 0.5 h / 60 °C / Inert atmosphere
3: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.08 h / 0 °C / Inert atmosphere; Darkness
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; triethylamine;
In
tetrahydrofuran; ethyl acetate;
2: Sonogashira coupling;
DOI:10.1021/ma101816z
- Guidance literature:
-
Multi-step reaction with 2 steps
1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / ethyl acetate / 0.5 h / 60 °C / Inert atmosphere
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.08 h / 0 °C / Inert atmosphere; Darkness
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; triethylamine;
In
tetrahydrofuran; ethyl acetate;
1: Sonogashira coupling;
DOI:10.1021/ma101816z
